Measurement evidence
Temperature effect on the synthesis of two Ni-MOFs with distinct performance in supercapacitor · Deng L., Qu H., Zhang Y. et al. · Journal of Solid State Chemistry · 2020 · 121026
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Green block crystals of compound 1 · Single Crystal
Room temperature to 1000 deg C, 5 deg C min-1, N2 atmosphere.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Overall mass loss | about 62.4% | — | — | Text Approximate | 5 · 3.5 Purity and stability · Fig. 4 |
| Initial water-loss mass decrease | 8.0% from 124-158 deg C | — | — | Text Exact Reported | 5 · 3.5 Purity and stability · Fig. 4 |
Orange block crystals of compound 2 · Single Crystal
Room temperature to 1000 deg C, 5 deg C min-1, N2 atmosphere.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Framework decomposition onset | beyond 300 deg C | — | — | Text Approximate | 5 · 3.5 Purity and stability · Fig. 4 |
| Ultimate residue | observed 20.3%, calculated 21.0%, attributed to NiO | — | — | Text Exact Reported | 5 · 3.5 Purity and stability · Fig. 4 |