Spectroscopy — Temperature effect on the synthesis of two Ni-MOFs with distinct performance in supercapacitor

Measurement evidence

Spectroscopy

Temperature effect on the synthesis of two Ni-MOFs with distinct performance in supercapacitor · Deng L., Qu H., Zhang Y. et al. · Journal of Solid State Chemistry · 2020 · 121026

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR spectroscopy with KBr pellets, 4000-400 cm-1, Nicolet 460

Green block crystals of compound 1 · Single Crystal

Used to assess carboxylate coordination and imidazole C-N vibrations.

Context
pristine framework
Measurement source
4-5 · 3.4 FT-IR spectra · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Carboxylate asymmetric-symmetric separationDelta nu = 238 cm-1 from peaks at 1590 and 1352 cm-1Text
Exact Reported
5 · 3.4 FT-IR spectra · Fig. S2

FT-IR spectroscopy with KBr pellets, 4000-400 cm-1, Nicolet 460

Orange block crystals of compound 2 · Single Crystal

Used to assess carboxylate coordination and imidazole C-N vibrations.

Context
pristine framework
Measurement source
4-5 · 3.4 FT-IR spectra · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Carboxylate asymmetric-symmetric separationDelta nu = 221 cm-1 from peaks at 1590 and 1369 cm-1Text
Exact Reported
5 · 3.4 FT-IR spectra · Fig. S2