Complete recipeSource: Main
Route 1: Other
p002-p003 · Synthesis Method
Metal precursors93 mg Ni(CH3COO)2.4H2O in 25 mL deionized water + 25 mL DMF
Linker precursors100 mg DDA in 50 mL DMF
SolventsDMF; deionized water
Atmospherenot specified
Temperature100
Time24
Oxidant / reductantoxidation of amino group mentioned as part of synthesis; separate oxidant not specified
Work-upcentrifuged, washed with deionized water and ethanol
Activationdried under vacuum at 70 degC
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Linker | DDA | 100 mg | p002-p003 · Synthesis Method |
| Solvent | N,N-dimethylformamide (DMF) | 50 mL for Solution A; 25 mL for Solution B | p002-p003 · Synthesis Method |
| Metal Source | Ni(CH3COO)2.4H2O | 93 mg | p002-p003 · Synthesis Method |
| Solvent | deionized water | 25 mL in Solution B; additional washing solvent | p002-p003 · Synthesis Method |
| Solvent | ethanol | washing solvent | p002-p003 · Synthesis Method |