Partial recipeSource: Main
Route 1: Hydrothermal
3 · Preparation of Cu-HHTT/CF · Fig. 1
Metal precursorsCu(CH3COO)2.H2O, amount reported only as 'a certain mass'
Linker precursorsHHTT (0.02 mmol, 7 mg)
Solventswater, 4 mL
Additives1 M HCl used for copper-foam pretreatment
Atmospherenot stated
Temperature85
Time12
Substrate orientationpre-treated copper foam placed in 20 mL glass bottle; orientation not stated
Work-upCopper foam ultrasonicated in 1 M HCl for 15 min, washed three times with water and ethanol; after reaction product washed three times with ethanol and water.
Activationdried at room temperature
Scalability contextAuthors describe the method as simple and fast, but no scale-up data are reported.
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Cu(CH3COO)2.H2O | a certain mass | 3 · Preparation of Cu-HHTT/CF · Fig. 1 |
| Linker | 2,3,6,7,14,15-hexahydroxytriptycene (HHTT) | 0.02 mmol, 7 mg | 3 · Preparation of Cu-HHTT/CF · Fig. 1 |
| Solvent | water | 4 mL | 3 · Preparation of Cu-HHTT/CF · Fig. 1 |
| Acid | HCl | 15 min ultrasonic pretreatment · 1 M | 3 · Preparation of Cu-HHTT/CF · Fig. 1 |
| Other | copper foam (CF) | not stated | 3 · Preparation of Cu-HHTT/CF · Fig. 1 |