Spectroscopy — A novel 2D conductive MOF nanobelts for highly efficient electrosynthesis of hydrogen peroxide

Measurement evidence

Spectroscopy

A novel 2D conductive MOF nanobelts for highly efficient electrosynthesis of hydrogen peroxide · Feng Q., Wang W., Yang X. et al. · Nano Research · 2025 · 94907439

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR and Raman spectroscopy

Ni-PTC-60 · Powder

FT-IR 400-4000 cm-1 on KBr pressed sheet; Raman with 532 nm diode laser.

Context
pristine powder
Measurement source
4 · 3.1 Synthesis and characterization of Ni-PTC · Figure 2d,e; Tables S2-S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-PTC-60 asymmetric COO- IR band1622 cm-1SI Table
Exact Reported
8 · Table S3 · Table S3
Ni-PTC-60 symmetric COO- IR band1395 cm-1SI Table
Exact Reported
8 · Table S3 · Table S3
Ni-PTC-60 Raman C-H band1311 cm-1SI Table
Exact Reported
8 · Table S3 · Table S3

X-ray photoelectron spectroscopy (XPS)

Ni-PTC-60 · Powder

ESCALAB 250Xi with monochromated Al Kalpha 150 W beam; binding energies corrected to C 1s C-C at 284.8 eV.

Context
pristine powder
Measurement source
1 · 2.1 Characterizations · Figure S2; Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-PTC-60 C 1s COO- binding energy288.6 eVText
Exact Reported
4 · 3.1 Synthesis and characterization of Ni-PTC · Figure 2a
Ni-PTC-60 XPS survey elementsNi, C, and O onlyText
Qualitative
4 · 3.1 Synthesis and characterization of Ni-PTC · Figure S2
Ni-PTC-60 Ni 2p1/2 binding energy874.3 eVSI Table
Exact Reported
8 · Table S1 · Table S1
Ni-PTC-60 Ni 2p3/2 binding energy856.6 eVSI Table
Exact Reported
8 · Table S1 · Table S1
Ni-PTC-60 O 1s COO- binding energy533.3 eVText
Exact Reported
4 · 3.1 Synthesis and characterization of Ni-PTC · Figure 2b