SEM and TEM
Fe-HHTP-MOF black microcrystalline powder · Powder
SEM at 2 kV after carbon coating; TEM at 300 kV after powder deposition on copper grid.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Mean crystallite angleMarked as a best value within this paper | Mean angle of 72 deg; table mean 72.294 deg | 72.294 deg | SD 3.336 deg | SI Table Exact Reported | SI p.5 · Statistical data of the crystallite angle · Table S1 |
| Crystallite size upper boundMarked as a best value within this paper | 300-500 nm | 500 nm | range upper bound | Caption Range | SI p.5 · Additional information · Figure S1 |
| Crystallite size lower bound | 300-500 nm | 300 nm | range lower bound | Caption Range | SI p.5 · Additional information · Figure S1 |