Porosity — An Electrically Conducting Three-Dimensional Iron–Catecholate Porous Framework

Measurement evidence

Porosity

An Electrically Conducting Three-Dimensional Iron–Catecholate Porous Framework · Mähringer et al. · Angewandte Chemie International Edition · 2021 · 18065-18072

1 measurement group · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Nitrogen adsorption/desorption and BET/QSDFT analysis

Fe-HHTP-MOF black microcrystalline powder · Powder

Autosorb 1 at 77.3 K with 99.99% N2; sample evacuated under high vacuum at 120 C for at least 12 h; AsiQwin v3.01 evaluation.

Temperature
77.3
Atmosphere
nitrogen
Geometry
Powder sorption sample
Context
pristine Fe-HHTP-MOF powder
Measurement source
18068 · Materials Characterization · Figure 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface areaMarked as a best value within this paper1490 m2 g^-11490 m2/gText
Exact Reported
18068 · Materials Characterization · Figure 3
Predicted Connolly surface area1675 m2 g^-11675 m2/gText
Exact Reported
18068 · Materials Characterization
Predicted Connolly pore volume1 cm3 g^-11 cm3/gText
Exact Reported
18068 · Materials Characterization
Low-pressure N2 uptakeup to 350 cm3 g^-1 at p/p0 < 0.1350 cm3/gup toText
Rounded Reported
18068 · Materials Characterization · Figure 3
QSDFT mean pore sizeMarked as a best value within this paper1.78 nm1.78 nmCaption
Exact Reported
18068 · Materials Characterization · Figure 3
Experimental pore volumeMarked as a best value within this paper0.7 cm3 g^-10.7 cm3/gText
Exact Reported
18068 · Materials Characterization · Figure 3