Microscopy Morphology — Electrochemical oxygen reduction catalysed by Ni3 (hexaiminotriphenylene)2

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ni3(HITP)2 thin film on glassy carbon electrode · Electrode

Tapping mode in air at room temperature; Gwyddion analysis.

Temperature: 296-298
Atmosphere: air
Geometry: film on electrode
Context: pristine framework film
Measurement source: main p.2 · Synthesis and quantification of Ni3(HITP)2 · Supplementary Fig. 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
GCE film thickness	about 120 nm	—	—	Text Approximate	main p.2 · Synthesis and quantification · Supplementary Fig. 1
ITO film thickness	about 300 nm	—	—	Text Approximate	main p.2 · Synthesis and quantification · Supplementary Fig. 1

Ni3(HITP)2 thin film on glassy carbon electrode · Electrode

SEM at 10 kV and 200k magnification before and after ORR on GC and ITO electrodes.

Geometry: films on GC and ITO electrodes
Context: pristine framework film before/after ORR
Measurement source: SI p.S9 · Supplementary Figure 10 · Supplementary Fig. 10

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
SEM morphology after O2 cycling	No perturbations in film morphology observed upon electrochemical cycling under O2.	—	—	Text Qualitative	main p.3 · Characterization before and after ORR · Supplementary Fig. 10