Spectroscopy — Electrical Conductivity in a Porous, Cubic Rare-Earth Catecholate

3 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Y6HOTP2 diffuse-reflectance heating sample · Powder

300-1200 nm spectra under dinitrogen; sample heated to 90 C for 12 h; spectra approximately every 20 min.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
New semiquinoid-associated diffuse-reflectance band	1000-1200 nm band appears on heating	—	range upper bound 1200 nm	Text Range	main p.6922 · Main text · Fig. 3

As-synthesised Eu6HOTP2 powder/crystals · Powder

Bruker ALPHA II, 64 scans, 4000-400 cm-1, 4 cm-1 resolution; dry nitrogen-filled glovebox.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Eu6HOTP2 ATR-IR spectrum collected	ATR-IR spectrum reported for Eu6HOTP2	—	—	Caption Qualitative	SI p.S6 · Figure S2 caption · Fig. S2

As-synthesised Y6HOTP2 powder/crystals · Powder

Bruker ALPHA II, 64 scans, 4000-400 cm-1, 4 cm-1 resolution; dry nitrogen-filled glovebox.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Y6HOTP2 ATR-IR spectrum collected	ATR-IR spectrum reported for Y6HOTP2	—	—	Caption Qualitative	SI p.S6 · Figure S2 caption · Fig. S2