cMOF Evidence Base
Diffraction Structure — Measuring and Reporting Electrical Conductivity in Metal-Organic Frameworks: Cd2(TTFTB) as a Case Study

Measurement evidence

Diffraction Structure

Measuring and Reporting Electrical Conductivity in Metal-Organic Frameworks: Cd2(TTFTB) as a Case Study · Sun L., Park S.S., Sheberla D. et al. · Journal of the American Chemical Society · 2016 · 14772-14782

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction

X-ray diffraction and scattering

Pressed pellet, direct-contact probe · Pellet

PXRD of as-synthesised crystals and pressed/electrically characterised samples; ambient conditions.

Atmosphere
ambient
Geometry
powder / pressed pellet samples
Context
pristine_framework
Measurement source
S1; S19 · Characterization methods · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Structure retained after pressing/electrical characterisationPXRD confirmed Cd2(TTFTB) retained its structure——Caption
Qualitative		S19 · Figure captions · Figure S2

single-crystal X-ray crystal indexing / structural assignment

Cd2(TTFTB) single crystals · Single Crystal

Diffraction-quality crystal mounted on Kapton loop with paratone-N oil; 100 K; Mo Kalpha radiation; Bruker APEX2 indexing.

Temperature
100
Atmosphere
not specified during diffraction
Geometry
single crystal on Kapton loop
Context
pristine_framework
Measurement source
S1; S18 · Characterization methods · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Long crystal axis assigned to crystallographic c axislong dimension coincides with crystallographic c axis——Text
Qualitative		p002 / 14773 · Introduction · Figure S1