Measurement evidence
Two-dimensional d-π conjugated metal-organic framework based on hexahydroxytrinaphthylene · Meng Z., Mirica K.A. · Nano Research · 2021 · 369-375
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
iodine-doped Cu3(HHTN)2 powder · Powder
Experimental PXRD pattern compared with pristine Cu3(HHTN)2 and elemental I2.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| iodine-doped PXRD retained [100] peak | 2theta = 3.5° | — | — | Text Rounded Reported | 16 · S11 I2 Doping Study of Cu3(HHTN)2 · Fig. S28 |
| iodine-doped PXRD retained [200] peak | 2theta = 7.0° | — | — | Text Rounded Reported | 16 · S11 I2 Doping Study of Cu3(HHTN)2 · Fig. S28 |
as-synthesised Cu3(HHTN)2 dark brown powder · Powder
PXRD used to confirm Cu3(HHTN)2 formation and compare experimental pattern with simulated slipped-parallel and staggered structures.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| interlayer spacing d001Marked as a best value within this paper | d001 = 3.29 Å | — | — | Text Exact Reported | 2 · 2.2 Structural characterization · Fig. 2b |
| optimised MOF synthesis yieldMarked as a best value within this paper | 75 mg, yield 87% based on formula Cu3(HHTN)2 | — | — | Text Exact Reported | 6 · S2.2 Synthesis of Cu3(HHTN)2 MOF · Table S1 |
| PXRD [100] peak | 2theta = 3.49° | — | — | Text Exact Reported | 2 · 2.2 Structural characterization · Fig. 2b |
| PXRD [200] peak | 2theta = 6.95° | — | — | Text Exact Reported | 2 · 2.2 Structural characterization · Fig. 2b |
| structural pore aperture from PXRDMarked as a best value within this paper | 2.5 nm | 25 angstrom | — | Text Rounded Reported | 2 · 2.2 Structural characterization · Scheme 1, Fig. 1 |