Microscopy Morphology — Imparting Functionality and Enhanced Surface Area to a 2D Electrically Conductive MOF via Macrocyclic Linker

Measurement evidence

Microscopy Morphology

Imparting Functionality and Enhanced Surface Area to a 2D Electrically Conductive MOF via Macrocyclic Linker · Pham H.T.B., Choi J.Y., Huang S. et al. · Journal of the American Chemical Society · 2022 · 10615-10621

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM/TEM particle-size analysis

Scanning electron microscopy Transmission electron microscopy

Cu-HHTC synthesised at 60 C · Powder

Cu-HHTC samples synthesised at 30, 40, 50 and 60 C; particle size calculated by multiplying short and long particle sides.

Geometry: Powder rods
Context: Pristine Cu-HHTC temperature series.
Measurement source: main p.4, article p.10618 · Particle Size Tunability · Figure 4b; Figures S17-S19

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

SEM, TEM and HR-TEM

Scanning electron microscopy Transmission electron microscopy

Pristine Cu-HHTC synthesised at 50 C for 8 h · Powder

TEM image and HR-TEM along [001] direction; SEM particle size distribution in SI.

Geometry: Powder rods
Context: Pristine Cu-HHTC framework.
Measurement source: main p.3, article p.10617 · Structure Characterization · Figure 2e; Figure S16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Average rod crystal size	average size of 256 nm	—	—	Text Rounded Reported	main p.3, article p.10617 · Structure Characterization · Figure S16
HR-TEM pore size	22 Angstrom	—	—	Text Rounded Reported	main p.3, article p.10617 · Structure Characterization · Figure 2e