Microscopy Morphology — Charge-Transfer-Induced Electrical Conductivity in a Tetrathiafulvalene-Based Metal-Organic Framework

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

activated Zn2TTFTB · Powder

Top-view powder micrographs on JEOL JSM-7500F FE-SEM with EDS system; SE images at 1 kV; samples not metal-coated.

Geometry: Powder SEM
Context: pristine_control
Measurement source: p009 / 2540 · Experimental Section - Scanning Electron Microscopy

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Morphology after TCNE infiltration	M2TTFTB crystallite morphology remains unchanged after TCNE infiltration	—	—	Text Qualitative	p003 / 2534 · Results and Discussion · Figure S17 cited
Pristine M2TTFTB crystallite particle size	1-30 um	—	—	Text Range	p003 / 2534 · Results and Discussion · Figure S17 cited

3: (TCNE)0.46@Zn2TTFTB · Powder

JEM NEOARM with cold FEG at 200 kV; crystalline products deposited on carbon-coated copper grids without solvent.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
STEM-EDS distribution of TCNE-related elements	Uniform distribution of TCNE throughout MOF crystals expected; no evidence for large inhomogeneities	—	—	Text Qualitative	p004 / 2535 · Results and Discussion · Figure 3; Figures S18-S24 cited