Diffraction Structure — A Microporous and Naturally Nanostructured Thermoelectric Metal-Organic Framework with Ultralow Thermal Conductivity

Measurement evidence

Diffraction Structure

A Microporous and Naturally Nanostructured Thermoelectric Metal-Organic Framework with Ultralow Thermal Conductivity · Sun L., Liao B., Sheberla D. et al. · Joule · 2017 · 168-177

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction with Bruker D8 Advance, theta/2theta Bragg-Brentano geometry, nickel-filtered Cu Kalpha radiation

X-ray diffraction and scattering

as-synthesised Ni3(HITP)2 powder · Powder

Thin layers on zero-background silicon crystal plate; background corrected with Bruker Diffrac.Suite EVA software.

Context: pristine Ni3(HITP)2 powder compared with desolvated powder, pressed pellet, and simulated pattern
Measurement source: p008 / article p.174 · Experimental Procedures · Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Broad PXRD peak assigned to (002) stacking	broad peak at 2theta = 27.3 deg	—	—	Text Rounded Reported	p004 / article p.170 · Results · Figure S1
Pressed pellet PXRD matches powder pattern	PXRD pattern of pressed pellets matched powder; structure retained after 1 GPa pressure treatment	—	—	Text Qualitative	p005 / article p.171 · Results · Figure S1