Measurement evidence
A Microporous and Naturally Nanostructured Thermoelectric Metal-Organic Framework with Ultralow Thermal Conductivity · Sun L., Liao B., Sheberla D. et al. · Joule · 2017 · 168-177
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
pressed pellet of Ni3(HITP)2 · Pellet
Beam voltage 3 kV; pellet morphology and grain boundaries inspected.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
as-synthesised Ni3(HITP)2 powder · Powder
Images acquired at 300 kV, electron dose 30-40 e/A^2, summed from up to 20 images at 0.2 s per image before visible damage.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Largest observed nanoparticle dimensions | 20 x 20 x 50 nm | — | — | Text Rounded Reported | p004 / article p.170 · Results · Figures 1B, 1C, S3 |
| Tubular pore width | 1.5 nm-wide tubular pores | — | — | Text Rounded Reported | p003 / article p.169 · Introduction · Figure 1A |
| Approximate stacked sheet count in largest particle | approximately 150 stacked sheets | — | — | Text Approximate | p004 / article p.170 · Results · Figure 1C |
| TEM/FFT hexagonal unit-cell a and b | a = b = 20.1 A | 2.01 nm | — | Text Rounded Reported | p004 / article p.170 · Results · Table S1 |
| TEM/FFT hexagonal unit-cell c | c = 6.6 A | 0.66 nm | — | Text Rounded Reported | p004 / article p.170 · Results · Table S1 |
| Observed FFT d-spacing, index 002 | 3.3 A | 0.33 nm | — | SI Table Exact Reported | SI p005 · Table S1 · Table S1 |
| Observed FFT d-spacing, index 100 | 17.4 A | 1.74 nm | — | SI Table Exact Reported | SI p005 · Table S1 · Table S1 |
| Observed FFT d-spacing, index 110 | 10.1 A | 1.01 nm | — | SI Table Exact Reported | SI p005 · Table S1 · Table S1 |
| Observed FFT d-spacing, index 200 | 8.5 A | 0.85 nm | — | SI Table Exact Reported | SI p005 · Table S1 · Table S1 |