powder X-ray diffraction
Co3HHTP2/graphite blended pellet · Pellet
scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
Measurement evidence
Drawing sensors with ball-milled blends of metal-organic frameworks and graphite · Ko M., Aykanat A., Smith M.K. et al. · Sensors (Switzerland) · 2017 · 2192
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Co3HHTP2/graphite blended pellet · Pellet
scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
pure Co3HHTP2 powder · Powder
powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| pure Co3HHTP2 pXRD 020 peak | 2theta = 9.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Co3HHTP2 pXRD 100 peak | 2theta = 4.5 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Co3HHTP2 pXRD 120 peak | 2theta = 12.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
Cu3HHTP2/graphite blended pellet · Pellet
scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu3HHTP2/graphite crystallinity after milling | retains crystallinity after ball-milling with graphite | — | — | Caption Qualitative | 13 of 17 · Supplementary materials caption · Figure S8 |
| graphite interplanar spacing in blends | 3.4 Angstrom | — | — | Text Exact Reported | 7 of 17 · Results 3.2 · Figure S8 |
| graphite (002) pXRD peak retained in all blends | 2theta = 26 deg; d = 3.4 Angstrom | — | — | Text Exact Reported | 7 of 17 · Results 3.2 · Figure S8 |
pure Cu3HHTP2 powder · Powder
powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| pure Cu3HHTP2 pXRD 020 peak | 2theta = 9.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Cu3HHTP2 pXRD 100 peak | 2theta = 4.5 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Cu3HHTP2 pXRD 120 peak | 2theta = 12.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
Fe3HHTP2/graphite blended pellet · Pellet
scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
pure Fe3HHTP2 powder · Powder
powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Fe3HHTP2 pXRD crystallinity | largely amorphous, with no distinct diffraction peaks | — | — | Qualitative Qualitative | 5-6 of 17 · Results 3.1 · Figure S8 |
Ni3HHTP2/graphite blended pellet · Pellet
scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni3HHTP2/G and Co3HHTP2/G MOF shear-plane attenuation | shear planes (100), (020), and (120) attenuated upon ball-milling | — | — | Caption Qualitative | 13 of 17 · Supplementary materials caption · Figure S8 |
pure Ni3HHTP2 powder · Powder
powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| pure Ni3HHTP2 pXRD 020 peak | 2theta = 9.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Ni3HHTP2 pXRD 100 peak | 2theta = 4.5 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |
| pure Ni3HHTP2 pXRD 120 peak | 2theta = 12.4 deg | — | — | Text Exact Reported | 5 of 17 · Results 3.1 · Figure S8 |