Diffraction Structure — Drawing sensors with ball-milled blends of metal-organic frameworks and graphite

Measurement evidence

Diffraction Structure

Drawing sensors with ball-milled blends of metal-organic frameworks and graphite · Ko M., Aykanat A., Smith M.K. et al. · Sensors (Switzerland) · 2017 · 2192

8 measurement groups · 14 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction

Co3HHTP2/graphite blended pellet · Pellet

scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk

Atmosphere
ambient
Geometry
blend powder/pellet
Context
MOF/graphite composite
Measurement source
7 of 17 · Results 3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

powder X-ray diffraction

pure Co3HHTP2 powder · Powder

powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2

Atmosphere
ambient
Geometry
powder
Context
pristine MOF control
Measurement source
5-7 of 17 · Results 3.1-3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
pure Co3HHTP2 pXRD 020 peak2theta = 9.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Co3HHTP2 pXRD 100 peak2theta = 4.5 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Co3HHTP2 pXRD 120 peak2theta = 12.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8

powder X-ray diffraction

Cu3HHTP2/graphite blended pellet · Pellet

scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk

Atmosphere
ambient
Geometry
blend powder/pellet
Context
MOF/graphite composite
Measurement source
7 of 17 · Results 3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu3HHTP2/graphite crystallinity after millingretains crystallinity after ball-milling with graphiteCaption
Qualitative
13 of 17 · Supplementary materials caption · Figure S8
graphite interplanar spacing in blends3.4 AngstromText
Exact Reported
7 of 17 · Results 3.2 · Figure S8
graphite (002) pXRD peak retained in all blends2theta = 26 deg; d = 3.4 AngstromText
Exact Reported
7 of 17 · Results 3.2 · Figure S8

powder X-ray diffraction

pure Cu3HHTP2 powder · Powder

powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2

Atmosphere
ambient
Geometry
powder
Context
pristine MOF control
Measurement source
5-7 of 17 · Results 3.1-3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
pure Cu3HHTP2 pXRD 020 peak2theta = 9.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Cu3HHTP2 pXRD 100 peak2theta = 4.5 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Cu3HHTP2 pXRD 120 peak2theta = 12.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8

powder X-ray diffraction

Fe3HHTP2/graphite blended pellet · Pellet

scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk

Atmosphere
ambient
Geometry
blend powder/pellet
Context
MOF/graphite composite
Measurement source
7 of 17 · Results 3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

powder X-ray diffraction

pure Fe3HHTP2 powder · Powder

powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2

Atmosphere
ambient
Geometry
powder
Context
pristine MOF control
Measurement source
5-7 of 17 · Results 3.1-3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Fe3HHTP2 pXRD crystallinitylargely amorphous, with no distinct diffraction peaksQualitative
Qualitative
5-6 of 17 · Results 3.1 · Figure S8

powder X-ray diffraction

Ni3HHTP2/graphite blended pellet · Pellet

scaled pXRD spectra for graphite, M3HHTP2 and M3HHTP2/graphite blend bulk

Atmosphere
ambient
Geometry
blend powder/pellet
Context
MOF/graphite composite
Measurement source
7 of 17 · Results 3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni3HHTP2/G and Co3HHTP2/G MOF shear-plane attenuationshear planes (100), (020), and (120) attenuated upon ball-millingCaption
Qualitative
13 of 17 · Supplementary materials caption · Figure S8

powder X-ray diffraction

pure Ni3HHTP2 powder · Powder

powder pattern compared with reported analysis and simulated configurations for Fe3HHTP2

Atmosphere
ambient
Geometry
powder
Context
pristine MOF control
Measurement source
5-7 of 17 · Results 3.1-3.2 · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
pure Ni3HHTP2 pXRD 020 peak2theta = 9.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Ni3HHTP2 pXRD 100 peak2theta = 4.5 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8
pure Ni3HHTP2 pXRD 120 peak2theta = 12.4 degText
Exact Reported
5 of 17 · Results 3.1 · Figure S8