Powder XRD and grazing-incidence XRD; Rietveld refinement
TCNQ@Cu3(BTC)2 powder · Powder
As-synthesised hydrated, activated, and TCNQ-infiltrated Cu3(BTC)2 powders and thin film
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Diagnostic guest-binding XRD peak | 2theta = 5.759 degrees | — | — | Text Exact Reported | 2 · main text · Fig. 1C |
| Cu3(BTC)2 lattice parameter | 2.617 +/- 0.001 nm | — | +/- 0.001 nm | Text Exact Reported | 2 · main text · Fig. 1C |
| TCNQ@Cu3(BTC)2 lattice parameter | 2.635 +/- 0.001 nm | — | +/- 0.001 nm | Text Exact Reported | 2 · main text · Fig. 1C; Fig. S2 |