Diffraction Structure — A Conductive 2D Conjugated Tetrathia[8]circulene-Based Nickel Metal–Organic Framework for Energy Storage

Measurement evidence

Diffraction Structure

A Conductive 2D Conjugated Tetrathia[8]circulene-Based Nickel Metal–Organic Framework for Energy Storage · Chang Z., Zhu M., Sun Y. et al. · Advanced Functional Materials · 2023 · 2301513

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD) and profile fitting

X-ray diffraction and scattering

as-synthesised Ni-TTC black powder · Powder

Rigaku MiniFlex 600, Cu sealed tube lambda = 1.54178 A at 40 kV and 15 mA; comparison with DFT simulated stacking models

Context: pristine framework powder
Measurement source: 2 · 2.1. Synthesis and Structural Characterization of Ni-TTC · Figure 1c; Figure S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
2D square lattice parameter from first five PXRD peaks	a = b = 14.46 A	—	—	Text Exact Reported	2 · 2.1. Synthesis and Structural Characterization of Ni-TTC · Figure 1c
profile-fitted monoclinic a	a = 13.06 A	—	—	Text Exact Reported	2 · 2.1. Synthesis and Structural Characterization of Ni-TTC · Figure 1c
PXRD profile fitting GoF	GoF = 1.40%	—	—	Text Exact Reported	2 · 2.1. Synthesis and Structural Characterization of Ni-TTC · Figure 1c; Figure S2