Diffraction Structure — Direct Electrodeposition of Electrically Conducting Ni3(HITP)2 MOF Nanostructures for Micro-Supercapacitor Integration

Measurement evidence

Diffraction Structure

Direct Electrodeposition of Electrically Conducting Ni3(HITP)2 MOF Nanostructures for Micro-Supercapacitor Integration · Behboudikhiavi S., Chanteux G., Babu B. et al. · Small · 2024 · 2401509

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction on scratched electrodeposited films

X-ray diffraction and scattering

Optimised pulsed potentiostatic Ni3(HITP)2 film from MeOH-DMSO bath · Thin Film

PXRD patterns compared for simulated, chemical reference, potentiodynamic, aqueous potentiostatic, organic continuous and organic pulsed deposits.

Temperature: room temperature/not specified
Atmosphere: ambient measurement; synthesis under specified bath atmosphere
Geometry: scratched film powders; STOE Stadi P with Mo Kalpha in SI methods, plotted as Cu Kalpha-equivalent figure labels in captions
Context: pristine Ni3(HITP)2 phase purity
Measurement source: 5-6 · Results and Discussion · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Direct electronic conductivity measurement in this paper	not reported for electrodeposited Ni3(HITP)2 films	—	absence after main and SI review	Qualitative Qualitative	1-10 · Full article review
Most crystalline aqueous potentiostatic deposition potentialMarked as a best value within this paper	0.5 V provided the most crystalline and uniform film	—	—	Text Rounded Reported	4 · Results and Discussion · Figure S4A
PXRD impurity peaks	No other diffraction peaks identified in deposits	—	qualitative absence statement	Text Qualitative	5 · Results and Discussion · Figure 3
PXRD phase assignment	all Bragg peaks assigned to simulated and bulk chemically synthesised Ni3(HITP)2 phase for potentiostatic/pulsed deposits	—	—	Text Qualitative	5 · Results and Discussion · Figure 3