Microscopy Morphology — Direct Electrodeposition of Electrically Conducting Ni3(HITP)2 MOF Nanostructures for Micro-Supercapacitor Integration

3 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pt@Ni3(HITP)2 core-shell nanowire network · Electrode

SEM of nanowire network and TEM image showing Pt core/Ni3(HITP)2 shell; SI Figure S9 compares 20 mC and 650 mC shell-growth charges.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Charge density for 55 nm shell growth	650 mC cm-2	0.65 C cm-2	—	Text Rounded Reported	6 · Results and Discussion · Figure 5A
Ni3(HITP)2 shell thickness on Pt nanowiresMarked as a best value within this paper	uniform shell-layer of 55 nm thickness	—	—	Text Rounded Reported	6 · Results and Discussion · Figure 5A

Interconnected Ni3(HITP)2 nanotube network · Electrode

Wide-view and high-resolution SEM plus TEM highlighting hollow Ni3(HITP)2 nanotube morphology.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Charge density for nanotube network deposition	about 2 C cm-2	—	about	Text Approximate	6 · Results and Discussion · Figure 5B
Ni3(HITP)2 nanotube scaffold network height	estimated at 15 um	—	estimated	Text Approximate	6 · Results and Discussion · Figure S10
Ni3(HITP)2 nanotube outer diameter	outer diameter of 230 nm	—	—	Text Rounded Reported	6 · Results and Discussion · Figure 5B
Ni3(HITP)2 nanotube wall thickness	70 nm wall thickness	—	—	Text Rounded Reported	6 · Results and Discussion · Figure 5B

Ni3(HITP)2 films on Pt, stainless steel, VN/Si/Si3N4, and carbon cloth · Thin Film

Optimised pulsed MeOH-DMSO deposition on Pt sheet, stainless steel, VN/Si/Si3N4, and carbon cloth.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni3(HITP)2 particle diameter on carbon cloth	200 to 300 nm in diameter on carbon cloth	—	200-300 nm	Text Range	6 · Results and Discussion · Figure 4D
Ni3(HITP)2 particle diameter on Pt sheet	reaching more than 2-3 um diameter on Pt sheet	—	>2-3 um	Text Range	6 · Results and Discussion · Figure 4A
Ni3(HITP)2 particle diameter on stainless steel	expanding to 1 um diameter on stainless-steel sheet	—	about/from text wording	Text Approximate	6 · Results and Discussion · Figure 4B
Ni3(HITP)2 particle diameter on VN current collector	nanoscopic spherical particles smaller than 200 nm	—	less than	Text Range	5 · Results and Discussion · Figure 4C