Spectroscopy — Preparation of Bimetallic Conductive Metal-organic Framework Material Ni/Co-CAT for Electrocatalytic Oxygen Reduction 双金属导电金属有机框架材料 Ni/Co-CAT 的制备及其氧还原催化性能研究

Measurement evidence

Spectroscopy

Preparation of Bimetallic Conductive Metal-organic Framework Material Ni/Co-CAT for Electrocatalytic Oxygen Reduction 双金属导电金属有机框架材料 Ni/Co-CAT 的制备及其氧还原催化性能研究 · Geng Y., Lin X., Sun Y. et al. · Acta Chimica Sinica · 2022 · 748-755

2 measurement groups · 16 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XPS

X-ray photoelectron spectroscopy

Ni-CAT powder · Powder

PHI5000 Versaprobe III, 200 W, Al Kα radiation.

Context: pristine Ni-CAT powder
Measurement source: 749-751, 754 · 2.1; 4.5 · Figure 2b,c

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni-CAT C 1s C=O binding energy	287.8 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2b
Ni-CAT C 1s C=C binding energy	284.3 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2b
Ni-CAT C 1s C-O binding energy	285.4 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2b
Ni-CAT Ni 2p1/2 binding energy	874.1 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2c
Ni-CAT Ni 2p3/2 binding energy	856.3 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2c

XPS

X-ray photoelectron spectroscopy

Ni-Co-CAT powder · Powder

PHI5000 Versaprobe III, 200 W, Al Kα radiation.

Context: pristine mixed-metal Ni-Co-CAT powder
Measurement source: 749-751, 754 · 2.1; 4.5 · Figure 2d-f

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni-Co-CAT C 1s C=O binding energy	288.1 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2d
Ni-Co-CAT C 1s C=C binding energy	284.5 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2d
Ni-Co-CAT C 1s C-O binding energy	285.7 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2d
Ni-Co-CAT Co 2p1/2 binding energy	797.1 eV	—	—	Text Exact Reported	750 · 2.1 · Figure 2f
Ni-Co-CAT Co 2p3/2 binding energy	781.5 eV	—	—	Text Exact Reported	750 · 2.1 · Figure 2f
Ni-Co-CAT Co satellite peak	786.4 eV	—	—	Text Exact Reported	750 · 2.1 · Figure 2f
Ni-Co-CAT Co satellite peak	802.6 eV	—	—	Text Exact Reported	750 · 2.1 · Figure 2f
Ni-Co-CAT Ni 2p1/2 binding energy	874.2 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2e
Ni-Co-CAT Ni 2p3/2 binding energy	855.9 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2e
Ni-Co-CAT Ni satellite peak	860.9 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2e
Ni-Co-CAT Ni satellite peak	881.1 eV	—	—	Text Exact Reported	749 · 2.1 · Figure 2e