Microscopy Morphology — Conductive 2D metal-organic framework for high-performance cathodes in aqueous rechargeable zinc batteries

2 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

as-synthesised Cu3(HHTP)2 powder / nanorods · Powder

FE-SEM at 20 kV and 20 uA; LD-HRTEM on JEOL Grand ARM at 300 kV using low electron dose.

Context: pristine framework
Measurement source: rendered pages 2, 4, and 8 / article pp.2, 4, and 8 · Results; Methods - Characterization and TEM · Figure 2; Supplementary Figs. 1 and 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
(100) crystal plane lattice distance along [010]	2.0 nm	—	—	Text Rounded Reported	rendered page 2 / article p.2 · Results - Synthesis and characterization · Figure 2g
Cu3(HHTP)2 nanorod maximum diameter	500 nm	—	—	Text Range	rendered page 2 / article p.2 · Results - Synthesis and characterization · Figure 2b
Cu3(HHTP)2 nanorod minimum diameter	20 nm	—	—	Text Range	rendered page 2 / article p.2 · Results - Synthesis and characterization · Figure 2b
Cu3(HHTP)2 nanorod diameter range	around 20-500 nm	—	—	Text Range	rendered page 2 / article p.2 · Results - Synthesis and characterization · Figure 2b; Supplementary Figs. 1-2
hexagonal pore diameter / d100	~2.0 nm	—	—	Caption Approximate	rendered page 4 / article p.4 · Figure 2 caption · Figure 2d

fully discharged Cu3(HHTP)2 electrode · Electrode

Fully discharged Cu3(HHTP)2 electrode; STEM-EDX maps C, Cu, O, and Zn; LD-HRTEM and SAD used for (100) interplanar distance.

Geometry: electrode
Context: fully discharged composite cathode
Measurement source: rendered pages 6 and 7 / article pp.6-7 · Confirmation of inserting Zn2+ ions · Figure 5b-f

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
discharged LD-HRTEM average d100	1.87 nm	—	—	Caption Exact Reported	rendered page 6 / article p.6 · Figure 5 caption · Figure 5c,d
SAD discharged (100) lattice distance	1.90(+/-0.01) nm	—	+/-0.01 nm	Text Exact Reported	rendered page 7 / article p.7 · Confirmation of inserting Zn2+ ions · Figure 5f
SAD pristine (100) lattice distance	2.01(+/-0.01) nm	—	+/-0.01 nm	Text Exact Reported	rendered page 7 / article p.7 · Confirmation of inserting Zn2+ ions · Figure 5e
Zn distribution in discharged electrode	uniform Zn distribution over the entire electrode area	—	—	Text Qualitative	rendered page 7 / article p.7 · Confirmation of inserting Zn2+ ions · Figure 5b