Diffraction Structure — Employing Triphenylene-Based, Layered, Conductive Metal-Organic Framework Materials as Electrochemical Sensors for Nitric Oxide in Aqueous Media

Measurement evidence

Diffraction Structure

Employing Triphenylene-Based, Layered, Conductive Metal-Organic Framework Materials as Electrochemical Sensors for Nitric Oxide in Aqueous Media · Ambrogi E.K., Li Y., Chandra P. et al. · ACS Sensors · 2025 · 553-562

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD of dropcast films after sonication

Ni3(HHTP)2 dropcast on glassy carbon electrode · Electrode

Dropcast HHTP MOF films after 5 h sonication compared with powder and simulated stacking patterns.

Geometry
dropcast MOF film on electrode substrate
Context
pristine dropcast films
Measurement source
S8 · Characterization of Dropcast HHTP MOF Films · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Dropcast film structure retentionMOFs retained crystalline structure and rod-like morphology after 5 h sonication.Text
Qualitative
555 · Characterization of HHTP MOFs · Figures S7-S11

Powder X-ray diffraction (PXRD)

Co3(HHTP)2 microcrystalline powder · Powder

Rigaku Miniflex, Cu Kalpha radiation; compared with simulated ABAB and AAAA stacking patterns.

Geometry
powder sample
Context
pristine powders; applies to Co, Ni, Cu and Zn powder samples
Measurement source
S2 · General Methods
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co3(HHTP)2 stacking assignmentABAB stacking pattern of alternating MOF and intercalated layersText
Qualitative
555 · Characterization of HHTP MOFs · Figure 1b
Cu3(HHTP)2 stacking assignmentAAAA-type stacking without intercalated layerText
Qualitative
555 · Characterization of HHTP MOFs · Figure 1c
Ni3(HHTP)2 stacking assignmentABAB stacking pattern of alternating MOF and intercalated layersText
Qualitative
555 · Characterization of HHTP MOFs · Figure 1b
Zn3(HHTP)2 stacking assignmentslipped-parallel/AAAA-like stacking similar to Cu3(HHTP)2Text
Qualitative
555 · Characterization of HHTP MOFs · Figure 1c