cMOF Evidence Base
Microscopy Morphology — Multiple-Hydrogen-Bond Approach to Uncommon Pd(III) Oxidation State: A Pd-Br Chain with High Conductivity and Thermal Stability

Measurement evidence

Microscopy Morphology

Multiple-Hydrogen-Bond Approach to Uncommon Pd(III) Oxidation State: A Pd-Br Chain with High Conductivity and Thermal Stability · Mian M.R., Iguchi H., Takaishi S. et al. · Journal of the American Chemical Society · 2017 · 6562-6565

1 measurement group · 1 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

scanning tunneling microscopy

Copper-luster rod-like single crystals of compound 3 · Single Crystal

Room temperature and ambient pressure; flat bc-plane surface exposed by cellophane tape; constant-height mode, JEOL JSPM-5200, Vs = +0.138 V, tunnel current 2.00 nA.

Temperature
room temperature
Atmosphere
ambient pressure
Geometry
bc-plane crystal surface; chain direction b axis
Context
pristine target crystal
Measurement source
SI p.S2 · Characterization and Instrumentation · Figure 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
STM bright-spot periodicity along chainapproximately every 5 A5 AngstromapproximatelyText
Approximate		main p.3, article p.6564 · STM electronic-state imaging · Figure 3a,c