Diffraction Structure — A Conductive Cu-Based Metal–Organic Framework Ribbon with High-Density Redox-Active Centers as Cathode for Stable High-Capacity Lithium-Ion Batteries

Measurement evidence

Diffraction Structure

A Conductive Cu-Based Metal–Organic Framework Ribbon with High-Density Redox-Active Centers as Cathode for Stable High-Capacity Lithium-Ion Batteries · Yang M., Wang Y., Huang Y.-F. et al. · Angewandte Chemie - International Edition · 2025 · e202421008

2 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD after chemical exposure

activated DDA-Cu MOF powder · Powder

Immersion in CH3OH, DMF, DCM, THF, 1 M HCl, 1 M NaOH, and 4 M LiTFSI in DOL/DME for 48 h

Context
pristine framework
Measurement source
4 · Results and Discussion · Figure S11
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD retention after chemical exposurecrystal structure maintained after solvent/electrolyte/acid/base immersion for 48 hText
Qualitative
4 · Results and Discussion · Figure S11

PXRD with Pawley refinement

activated DDA-Cu MOF powder · Powder

Powder X-ray diffraction, Cu Kalpha irradiation; simulated and experimental pattern comparison

Context
pristine framework
Measurement source
2 · Results and Discussion · Figure 1b-c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
lattice parameter a11.8 AText
Rounded Reported
2 · Results and Discussion · Figure 1b-c
lattice parameter b7.9 AText
Rounded Reported
2 · Results and Discussion · Figure 1b-c
lattice parameter c3.2 AText
Rounded Reported
2 · Results and Discussion · Figure 1b-c
lattice parameter gamma87.7 degText
Rounded Reported
2 · Results and Discussion · Figure 1b-c
interlayer distanceapproximately 3.2 AText
Approximate
2 · Results and Discussion · Figure 1b-c
assigned PXRD peaks7.32, 11.2, 22.7, and 27.9 deg assigned to (100), (010), (020), and (001)Text
Rounded Reported
2 · Results and Discussion · Figure 1b
Pawley Rp2.73 %Text
Rounded Reported
2 · Results and Discussion · Figure 1b-c
Pawley Rwp4.45 %Text
Rounded Reported
2 · Results and Discussion · Figure 1b-c
space groupP2/mText
Exact Reported
2 · Results and Discussion · Figure 1b-c