Diffraction Structure — Dominant Role of Hole Transport Pathway in Achieving Record High Photoconductivity in Two-Dimensional Metal–Organic Frameworks

Measurement evidence

Diffraction Structure

Dominant Role of Hole Transport Pathway in Achieving Record High Photoconductivity in Two-Dimensional Metal–Organic Frameworks · Wang D., Ostresh S., Streater D. et al. · Angewandte Chemie - International Edition · 2023 · e202309505

3 measurement groups · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

powder X-ray diffraction with Rietveld refinement

Cu-HHTP dried powder · Powder

Rigaku Miniflex II, Cu K alpha; experimental and simulated PXRD compared with AA/AB stacking models.

Context
pristine Cu-HHTP
Measurement source
p002 · Results and Discussion · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld axial microstrain55.2k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1a inset
Rietveld crystallite size124.8 nmVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1a inset
Rietveld equatorial microstrain49.8k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1a inset
interlayer distance from (002) stackingabout 3.2 AngstromText
Approximate
p002 · Results and Discussion · Figure 1
common PXRD peaknear 4.7 deg 2thetaText
Approximate
p002 · Results and Discussion · Figure 1
common PXRD peaknear 9.5 deg 2thetaText
Approximate
p002 · Results and Discussion · Figure 1
common PXRD peaknear 12.6 deg 2thetaText
Approximate
p002 · Results and Discussion · Figure 1

powder X-ray diffraction with Rietveld refinement

Cu/Zn-HHTP dried powder · Powder

Same PXRD/Rietveld workflow as Cu-HHTP.

Context
mixed-metal control
Measurement source
p002 · Results and Discussion · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld axial microstrain30.4k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1b inset
Rietveld crystallite size164.4 nmVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1b inset
Rietveld equatorial microstrain37.4k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1b inset

powder X-ray diffraction with Rietveld refinement

Zn-HHTP dried powder · Powder

Same PXRD/Rietveld workflow as Cu-HHTP.

Context
Zn control
Measurement source
p002 · Results and Discussion · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld axial microstrain22.8k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1c inset
Rietveld crystallite size87.1 nmVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1c inset
Rietveld equatorial microstrain27.5k microstrainVisual Estimate
Approximate
p002 · Results and Discussion · Figure 1c inset