cMOF Evidence Base
Diffraction Structure — Why conductivity is not always king-physical properties governing the capacitance of 2D metal-organic framework-based EDLC supercapacitor electrodes: A Ni3(HITP)2case study

Measurement evidence

Diffraction Structure

Why conductivity is not always king-physical properties governing the capacitance of 2D metal-organic framework-based EDLC supercapacitor electrodes: A Ni3(HITP)2case study · Borysiewicz M.A., Dou J.-H., Stassen I. et al. · Faraday Discussions · 2021 · 298-304

3 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction using Bruker D8 Advance, theta/2theta Bragg-Brentano geometry, Cu Kalpha anode (lambda = 1.5405 A).

X-ray diffraction and scattering

HITP_A Ni3(HITP)2 powder batch · Powder

Dry powder on zero-background silicon (510) plate.

Context
Pristine powder batch.
Measurement source
SI p.S1 · Characterization · Fig. 1b; Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD I100/I001 intensity ratioMarked as a best value within this paper13.7——Table
Exact Reported		main p.2, article p.299 · Main text · Table 1

Powder X-ray diffraction using Bruker D8 Advance, theta/2theta Bragg-Brentano geometry, Cu Kalpha anode (lambda = 1.5405 A).

X-ray diffraction and scattering

HITP_B Ni3(HITP)2 powder batch · Powder

Dry powder on zero-background silicon (510) plate.

Context
Pristine powder batch.
Measurement source
SI p.S1 · Characterization · Fig. 1b; Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD I100/I001 intensity ratio2.9——Table
Exact Reported		main p.2, article p.299 · Main text · Table 1

Powder X-ray diffraction using Bruker D8 Advance, theta/2theta Bragg-Brentano geometry, Cu Kalpha anode (lambda = 1.5405 A).

X-ray diffraction and scattering

HITP_C Ni3(HITP)2 powder batch · Powder

Dry powder on zero-background silicon (510) plate.

Context
Pristine powder batch.
Measurement source
SI p.S1 · Characterization · Fig. 1b; Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD I100/I001 intensity ratio1.8——Table
Exact Reported		main p.2, article p.299 · Main text · Table 1