Other — Effect on Schottky behaviour of 1D coordination polymers by altering para-substituents on benzoate ligands

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Compound 1 yellow block crystals · Single Crystal

30-800 degrees C under nitrogen, heating rate 12 degrees C min^-1.

Atmosphere: N2
Context: pristine framework
Measurement source: 13972; 13975-13976 · Materials and physical method; TGA and PXRD · Fig. S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
decomposition onset lower bound	decomposed above 200 degrees C	—	reported as above threshold	Text Approximate	13975-13976 · TGA and PXRD · Fig. S5
initial lattice methanol loss endpoint	up to 150 degrees C	—	endpoint phrased as up to	Text Approximate	13975-13976 · TGA and PXRD · Fig. S5
calculated ZnO residue	20.54%	—	—	Text Exact Reported	13976 · TGA and PXRD · Fig. S5
experimental ZnO residue	19.22%	—	—	Text Exact Reported	13976 · TGA and PXRD · Fig. S5

Compound 2 yellow block crystals · Single Crystal

30-800 degrees C under nitrogen, heating rate 12 degrees C min^-1.

Atmosphere: N2
Context: pristine framework
Measurement source: 13972; 13975-13976 · Materials and physical method; TGA and PXRD · Fig. S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
decomposition onset lower boundMarked as a best value within this paper	decomposed above 250 degrees C	—	reported as above threshold	Text Approximate	13976 · TGA and PXRD · Fig. S5
lattice methanol loss range	50-150 degrees C	—	—	Text Range	13976 · TGA and PXRD · Fig. S5
calculated ZnO residue	17.87%	—	—	Text Exact Reported	13976 · TGA and PXRD · Fig. S5
experimental ZnO residue	16.55%	—	—	Text Exact Reported	13976 · TGA and PXRD · Fig. S5