Spectroscopy — Photodimerization of a 1D Ladder Polymer through Single-Crystal to Single-Crystal Transformation Has an Effect on Electrical Conductivity

Measurement evidence

Spectroscopy

Photodimerization of a 1D Ladder Polymer through Single-Crystal to Single-Crystal Transformation Has an Effect on Electrical Conductivity · Islam S., Datta J., Maity S. et al. · Crystal Growth and Design · 2019 · 4057-4062

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Elemental analysis, FT-IR in KBr, and 1H NMR in d6-DMSO at 300 MHz and 298 K

Compound 1 colourless block crystals · Single Crystal

As-synthesised compound 1 characterised by elemental analysis, IR, and solution 1H NMR.

Temperature
298 for NMR
Context
pristine compound 1
Measurement source
p002 / article p.4058 · Experimental Section - Syntheses of Compounds
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
compound 1 isolated yield0.097 g, yield 70%Text
Rounded Reported
p002 / article p.4058 · Experimental Section - Syntheses of Compounds

Elemental analysis, FT-IR in KBr, and 1H NMR in d6-DMSO at 300 MHz and 298 K

Compound 2 light yellow photodimerised block crystals · Single Crystal

UV-photodimerised compound 2 characterised by elemental analysis, IR, and solution 1H NMR.

Temperature
298 for NMR
Context
photodimerised compound 2
Measurement source
p002 / article p.4058 · Experimental Section - Syntheses of Compounds
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
photodimerisation conversionformation of 100% dimerized productsText
Exact Reported
p003 / article p.4059 · Results and Discussion - Structural Descriptions · Figures S7-S8 referenced