Solution and solid-state NMR measurements.
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2026 · Intrinsically Conductive π-d Conjugated Layers with Co–N4 Active Sites for Efficient Nitrate Electrocatalysis and Zinc-Nitrate Batteries
Co3(HITP)2 drop-cast carbon paper electrode · Electrode · 14N and 15N-labelled nitrate sources; Bruker Avance 400 MHz NMR used to identify ammonium isotopologues.
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-201 powder · Powder · coordination-bond confirmation for Rh-isocyano MOFs
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-202 powder · Powder · coordination-bond confirmation for Rh-isocyano MOFs
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-203 powder · Powder · coordination-bond confirmation for Rh-isocyano MOFs
2025 · Development of an electrochemiluminescence aptasensor combining covalent-triazine framework emitter with exonuclease III-driven DNA walker for sensitive CEA detection
purified CTF powder · Powder · Chemical structure confirmation of imine-linked CTF; FT-IR and NMR spectra reported in SI Fig. S1.
2025 · Electrically Conducting Redox-Complementary Dual-Ligand 2D Graphitic MOF with Orthogonal Charge Transport Pathways
CDL-MOF1 microcrystalline black powder · Powder · Dried black powder dissolved in DMSO-d6 with a drop of CF3CO2D; Bruker 500 MHz NMR spectrometer.
2025 · Fabrication of a Novel Cu Based Conjugated Coordination Polymer for Effective Electroreduction of Nitrate to Ammonia and Zn–Nitrate Batteries
Cu3(HITP)2/CF pine-like electrode · Electrode · NRA electrolytes adjusted to pH 3 with 4 M H2SO4; D2O added; Bruker AVANCE III HD 400 MHz NMR.
2025 · Modulating the redox states in a 3D conductive MOF for sweat ascorbic acid monitoring
I2@FeTHQ/ITO working electrode · Electrode · Reaction mixture extracted from AA sensing system
2025 · Solvent-Directed Assembly of π-Stacked 3D Metal-Organic Frameworks with Tunable Conductivity Enhanced by C60 Encapsulation
NU-4003 · Single Crystal · D2SO4 digestion, DMSO-d6 solvent, mesitylene internal standard; estimates missing-linker defects for NU-4000-NU-4003
2025 · Tuning the dxy Orbital Energy Level in 2D Cobalt-Organic-Framework via in-Plane Conjugated Phthalocyanine for Self-Powered Sensing
2D MOF@Pc nanosheets · Nanosheet · Chemical/electronic structure comparison between 2D MOF and 2D MOF@Pc.
2024 · Naphthalene Diimide-Based Hydrogen-Bonded Organic Framework for High Electrical Conductivity and Ammonia Sensor Applications
Device A pristine drop-cast NDI(CPOH)2-SC · Single Crystal · grown non-doped single crystals dissolved in deuterated chloroform; NDI:DMF guest ratio from peak integrals
2024 · Photocatalytic Hydrogen Peroxide Production through Functionalized Semiconductive Metal-Organic Frameworks
EFB-MOF powder · Powder · 5 mg sample digested in D2O/DCl; linker-to-pillar ratio from integrations.
2024 · Reaction-Type-Dependent Behavior of Redox-Hopping in MOFs─Does Charge Transport Have a Preferred Direction?
Ru-NU-1000 particles · Powder · ~3 mg Ru-NU-1000 digested with ~5 drops concentrated H2SO4 in 600 uL d6-DMSO; heated at 80 C for 1 h, cooled, sonicated, and measured by 1H NMR.
2024 · Redox-active conductive metal-organic framework with high lithium capacities at low temperatures
SKIER-5 cyan solid powder · Powder · Ni K-edge XAFS at room temperature at 1D KIST-PAL; XPS with Al K-alpha source under 7e-8 Torr
2024 · Solid-State Electrochemical Carbon Dioxide Capture by Conductive Metal-Organic Framework Incorporating Nickel Bis(diimine) Units
Ni(DIB)2 solution electrochemical control · Unknown · Reduced Ni(DIB)2 prepared in H-cell; CO2-purged samples diluted in DMSO-d6 for NMR; MOF after 13CO2 capture measured by 13C ssNMR.
2023 · A Pyrazine-Based 2D Conductive Metal-Organic Framework for Efficient Lithium Storage†
HCl digestion product of TPQG-Cu-MOF · Powder · HCl digestion product compared with TPQ-8OH and TPQG-8OH.
2023 · A simplistic approach for the synthesis of Covalent Organic Frameworks(COFs) comprising of tetrafunctionalized porphyrin and polyoxometalates to uncover catalytic applications
P@Cu-AndCOF bulk solid · Powder · 1H NMR in DMSO-d6; FT-IR in KBr; UV-vis in DMF/CH3CN (v/v = 1:1).
2023 · A simplistic approach for the synthesis of Covalent Organic Frameworks(COFs) comprising of tetrafunctionalized porphyrin and polyoxometalates to uncover catalytic applications
P@Ni-AndCOF bulk solid · Powder · 1H NMR in DMSO-d6; FT-IR in KBr; UV-vis in DMF/CH3CN (v/v = 1:1).
2023 · A Triptycene-Based 2D MOF with Vertically Extended Structure for Improving the Electrocatalytic Performance of CO2 to Methane
2D-vc-MOF(Cu) glassy carbon working electrode · Electrode · Two-compartment H-cell, Nafion-117 membrane, CO2-saturated 0.1 M KCl, Pt counter, Ag/AgCl reference; CO2 continuously purged.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc pristine · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiBr (MOF:LiBr = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiCl (MOF:LiCl = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiI (MOF:LiI = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiBr (MOF:LiBr = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiCl (MOF:LiCl = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiI (MOF:LiI = 1:1) · Pellet · Powder sample loaded into NMR tube; kept at 298 K, 95% RH for one day and capped; PFG strength varied in 16 steps from 0 to 25 T m^-1; unidirectional model selected by authors.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiBr (MOF:LiBr = 1:1) · Pellet · Approximate comparison assuming anion self-diffusion nearly zero; Figure S17 plots 1H and 7Li transference numbers vs temperature.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiCl (MOF:LiCl = 1:1) · Pellet · Approximate comparison assuming anion self-diffusion nearly zero; Figure S17 plots 1H and 7Li transference numbers vs temperature.
2023 · Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides
Ti-dobdc-LiI (MOF:LiI = 1:1) · Pellet · Approximate comparison assuming anion self-diffusion nearly zero; Figure S17 plots 1H and 7Li transference numbers vs temperature.
2023 · Double advantages of 2D coordination polymer of coumarinyl-pyridyl Schiff base decorated Zn(II): The fabrication of Schottky device and Anti-carcinogenic activity
QPR light-brown crystalline ligand · Single Crystal · Ligand characterisation after Schiff-base synthesis; NMR in DMSO-d6.
2023 · Electrically conductive [Fe4S4]-based organometallic polymers
[Fe4S4Cl2(Me-NHC)] (1) powder · Powder · NMR in 20% DCl/D2O in DMSO-d6 in air; CHN under N2.
2023 · Electrically Conductive π-Intercalated Graphitic Metal-Organic Framework Containing Alternate π-Donor/Acceptor Stacks
iGMOF1 black powder · Powder · Composition and electronic-structure characterisation of iGMOF1, Cu3(HATP)2, HCTP-treated Cu3(HATP)2, and [HATP/HCTP]n array.
2023 · Linker-Based Bandgap Tuning in Conductive MOF Solid Solutions
Cu3(HAB)(TATHB) · Pellet · 5 mg sample digested in 0.4 mL D2O and 0.1 mL DCl (20 wt% in D2O), sonicated until dissolved; room-temperature 1H NMR.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@HKUST-1 particles · Powder · 4.0 mm solid-state NMR probe at 233.2 MHz; samples packed under Ar; T1 fitted by Equation S4.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@Mg-MOF-74 particles · Powder · 4.0 mm solid-state NMR probe at 233.2 MHz; samples packed under Ar; T1 fitted by Equation S4.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@MOF-5 particles · Powder · 4.0 mm solid-state NMR probe at 233.2 MHz; samples packed under Ar; T1 fitted by Equation S4.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@Zn-MOF-74 particles · Powder · 4.0 mm solid-state NMR probe at 233.2 MHz; samples packed under Ar; T1 fitted by Equation S4.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@Zn-MOF-74/Li-IL electrolyte pellet, 1:1.5 · Pellet · 4.0 mm solid-state NMR probe at 233.2 MHz; samples packed under Ar; T1 fitted by Equation S4.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@HKUST-1 particles · Powder · Li@MOF particles dissolved with DCl in DMSO-d6; FEC internal standard used to quantify LiTFSI and DME.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@Mg-MOF-74 particles · Powder · Li@MOF particles dissolved with DCl in DMSO-d6; FEC internal standard used to quantify LiTFSI and DME.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@MOF-5 particles · Powder · Li@MOF particles dissolved with DCl in DMSO-d6; FEC internal standard used to quantify LiTFSI and DME.
2023 · Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties
Li@Zn-MOF-74 particles · Powder · Li@MOF particles dissolved with DCl in DMSO-d6; FEC internal standard used to quantify LiTFSI and DME.
2022 · A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls
Y/Eu-MOF crystalline catalyst · Single Crystal · Y/Eu-MOF 0.5 mol%, carbonyl compound 0.25 mmol, TMSCN 34 uL/0.275 mmol/1.1 equiv, solvent-free, room temperature, N2, 24 h unless otherwise noted.
2022 · A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls
Y/Eu-MOF crystalline catalyst · Single Crystal · Monitored Y/Eu-MOF plus HBpin under catalytic conditions; also tested acetophenone hydroboration with BH3.THF instead of HBpin.
2022 · A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls
Y/Eu-MOF crystalline catalyst · Single Crystal · Acetophenone 28 uL/0.25 mmol and HBPin 40 uL/0.275 mmol in 0.5 mL solvent or solvent-free, room temperature, N2, 24 h.
2022 · A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls
Y/Eu-MOF crystalline catalyst · Single Crystal · Y/Eu-MOF 0.5 mol%, ketone 0.25 mmol, HBpin 40 uL/0.275 mmol/1.1 equiv, solvent-free, room temperature, N2; hydrolysis with 0.1 M NaOH and Et2O.
2022 · A novel Sn-based coordination polymer with high-efficiency and ultrafast lithium storage
as-prepared Sn-DHTPA powder · Powder · Bruker Avance III 600 MHz; 4.5 us 90 degree pulse; 10 k scans; 12 k spin frequency; referenced to SnCl4 at -158 ppm
2022 · Atomically Precise Integration of Multiple Functional Motifs in Catalytic Metal-Organic Frameworks for Highly Efficient Nitrate Electroreduction
In8 catalyst ink on carbon paper electrode · Electrode · H-type cell, Nafion 211 membrane, H2SO4 pH 1-5, KNO3 0.5-50 g L-1, Ar purge, typically -0.7 V vs RHE for 1 h.
2022 · Conductive Metal-Organic Frameworks Bearing M−O4 Active Sites as Highly Active Biomass Valorization Electrocatalysts
Co-CAT-Carbon Paper · Electrode · 10 mM HMF in 1 M KOH; Co-CAT on carbon paper; 1.42 V vs RHE; products quantified by NMR with internal standard.
2022 · Conductive Metal-Organic Frameworks Bearing M−O4 Active Sites as Highly Active Biomass Valorization Electrocatalysts
Ni-CAT-Carbon Paper · Electrode · 10 mM HMF in 1 M KOH; Ni-CAT on carbon paper; 1.42 V vs RHE unless otherwise specified; products quantified by NMR with internal standard.
2022 · Conductive Metal-Organic Frameworks Bearing M−O4 Active Sites as Highly Active Biomass Valorization Electrocatalysts
Co-CAT-Carbon Paper · Electrode · 5 mM HMF; Co-CAT; 1.12 V vs RHE; 5 days electrolysis.
2022 · From 2D to 3D: Postsynthetic Pillar Insertion in Electrically Conductive MOF
Cu-THQ-BPY, Cu2+:BPY feed ratio 1:1 · Powder · 5 mg sample digested in 0.5 mL D2O and 0.1 mL HCl (20 wt% in D2O), filtered through 0.45 um nylon membrane; Bruker AV-III 300 MHz.
2022 · Generation of Environmentally Persistent Free Radicals on Metal-Organic Frameworks
MIL-100(Al) powder · Powder · Bruker Ascend 700 MHz, resonance frequency 182.44 MHz; precursor-dosed samples activated under vacuum at 150 C for 12 h before NMR.
2022 · Highly Effective Generation of Singlet Oxygen by an Imidazole-Linked Robust Photosensitizing Covalent Organic Framework
as-synthesized PyPor-COF powder · Powder · PyPor-COF compared with model compound.
2022 · Host-guest molecular interaction promoted urea electrosynthesis over a precisely designed conductive metal-organic framework
Co-PMDA-2-mbIM electrode on carbon cloth · Electrode · 0.1 M KHCO3, 15N2 feed, H-type cell, Co-PMDA-2-mbIM electrode; potentials varied, optimum -0.5 V vs RHE.
2022 · Host-guest molecular interaction promoted urea electrosynthesis over a precisely designed conductive metal-organic framework
Co-PMDA-2-mbIM electrode on carbon cloth · Electrode · 0.1 M KHCO3, purified N2 + CO2 feed, chronoamperometry from -0.3 to -0.7 V vs RHE for 2 h; best at -0.5 V vs RHE.
2022 · Metal-Organic Framework Assembled on Oriented Nanofiber Arrays for Field-Effect Transistor and Gas Sensor-Based Applications
oriented PDMS-PCDA/Cu NFAs · Thin Film · PDMS-PCDA ligand characterised in CDCl3; solvent signals used as internal standards.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
Purified HHTP plus 0.3 equiv 2,5-dichloro-1,4-benzoquinone · Model · 1:1 d6-DMSO/D2O with dimethyl sulfone reference after 0.3 equiv 2,5-dichloro-1,4-benzoquinone addition.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
Acros HHTP batch 1 · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
Acros HHTP batch 2 · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
Purified HHTP · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
Purified HHTP plus 0.3 equiv 2,5-dichloro-1,4-benzoquinone · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
TCI HHTP batch 1 · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework
TCI HHTP batch 2 · Model · HHTP wt% by quantitative NMR; water wt% by TGA where applicable.
2022 · Probing the electronic and ionic transport in topologically distinct redox-active metal-organic frameworks in aqueous electrolytes
CAU-24 powder · Powder · Digested CAU-24 samples with and without HCl/DMF heating step compared to assess coordinated benzoate removal.
2022 · Synthesis and Characterization of Schiff Base Polymers via Metal Coordination and Its Application in Infrared Stealth Coating
D230-PyAL coating/polymer · Thin Film · 1H NMR in CDCl3 at 300 K; UV-Vis used to determine optical band gap; FTIR/XPS used for structure assignment
2021 · Conjugated crosslinks boost the conductivity and stability of a single crystalline metal-organic framework
activated ZrBPD-4F4TS-Ox · Powder · activated ZrBPD-4F4TS and activated ZrBPD-4F4TS-Ox comparison
2021 · Heterometallic Actinide-Containing Photoresponsive Metal-Organic Frameworks: Dynamic and Static Tuning of Electronic Properties
TCNQ@Th-MOF · Powder · TCNQ molecules per pore determined from digested samples.
2021 · Heterometallic Actinide-Containing Photoresponsive Metal-Organic Frameworks: Dynamic and Static Tuning of Electronic Properties
TCNQ@Zr-65% powder · Powder · TCNQ molecules per pore determined from digested samples.
2021 · Mimicking the Electron Transport Chain and Active Site of [FeFe] Hydrogenases in One Metal-Organic Framework: Factors That Influence Charge Transport
PCN-700_NDI_ta powder · Powder · Approximately 5 mg MOF digested in 0.55 mL DMSO-d6 plus 0.05 mL 35% DCl in D2O and sonicated at least 20 min.
2021 · MOF matrix isolation: Cooperative conformational mobility enables reliable single crystal transformations
MnMOF-1-ace · Single Crystal · 1H NMR of digested MOF samples monitored exchange from DMF to acetone and from acetone to DEE, DCM, THF and p-xylene over 90 min.
2021 · Promoting ethylene production over a wide potential window on Cu crystallites induced and stabilized via current shock and charge delocalization
Stand-alone Cu3(HITP)2 CO2RR electrode · Electrode · 0.1 M KHCO3, CO2-saturated, stand-alone Cu3(HITP)2 comparison.
2021 · Promoting ethylene production over a wide potential window on Cu crystallites induced and stabilized via current shock and charge delocalization
KB@Cu3(HITP)2 CO2RR electrode · Electrode · 0.1 M KHCO3, CO2-saturated, Ag/AgCl reference converted to RHE, glassy carbon working electrode, CO2 flow 20 cm3 min-1.
2021 · The Origins of Ion Conductivity in MOF-Ionic Liquids Hybrid Solid Electrolytes
MIL-121 + IL + LiTFSI · Pellet · Bruker Avance III 300; 7.0 T; 116.59 MHz for 7Li; 90 degree pulses 2-3 us; 10 s recycle delay; 128 FIDs; Duran tubes fire sealed
2021 · The Origins of Ion Conductivity in MOF-Ionic Liquids Hybrid Solid Electrolytes
MIL-121/Li + IL · Pellet · Bruker Avance III 300; 7.0 T; 116.59 MHz for 7Li; 90 degree pulses 2-3 us; 10 s recycle delay; 128 FIDs; Duran tubes fire sealed
2021 · The Origins of Ion Conductivity in MOF-Ionic Liquids Hybrid Solid Electrolytes
MIL-121/Li + IL + LiTFSI · Pellet · Bruker Avance III 300; 7.0 T; 116.59 MHz for 7Li; 90 degree pulses 2-3 us; 10 s recycle delay; 128 FIDs; Duran tubes fire sealed
2021 · The Origins of Ion Conductivity in MOF-Ionic Liquids Hybrid Solid Electrolytes
MIL-121/Li + IL + LiTFSI · Pellet · Supplementary comparison of normalised 7Li NMR intensities at 21 deg C for Li-containing samples and at 100 deg C for lithium/ionic-liquid samples.
2020 · A Light-Responsive Metal–Organic Framework Hybrid Membrane with High On/Off Photoswitchable Proton Conductivity
Synthesised sulfated spiropyran / SSP · Powder · NMR spectra at 293 K comparing thermal equilibrium MC state and SP form after sufficient visible-light irradiation.
2020 · Colloidal crystal engineering with metal–organic framework nanoparticles and DNA
Ag+-stabilized PCN-222 2D superlattice photocatalyst · Powder · Product selectivity after CEES photooxidation checked against CEES, CEESO and CEESO2 spectra.
2020 · Electrically Conductive 3D Metal-Organic Framework Featuring π-Acidic Hexaazatriphenylene Hexacarbonitrile Ligands with Anion-πInteraction and Efficient Charge-Transport Capabilities
Free HATHCN ligand powder/crystals · Powder · Ligand identity checks reported in SI after literature synthesis.
2020 · Highly Selective CO2 Electroreduction to CH4 by In Situ Generated Cu2O Single-Type Sites on a Conductive MOF: Stabilizing Key Intermediates with Hydrogen Bonding
Cu2O@CuHHTP, -1.2 V 30 min · Electrode · 0.1 M KCl/0.1 M KHCO3, CO2-saturated pH 6.8, CO2 flow 30 sccm, Nafion-117 membrane, Ag/AgCl reference, Pt foil counter, potentials vs RHE without IR compensation
2020 · Highly Selective CO2 Electroreduction to CH4 by In Situ Generated Cu2O Single-Type Sites on a Conductive MOF: Stabilizing Key Intermediates with Hydrogen Bonding
Cu2O@CuHHTP, -1.2 V 30 min · Electrode · CO2-saturated 0.1 M KCl/0.1 M KHCO3; potentials vs RHE without IR compensation
2020 · Single-Site, Single-Metal-Atom, Heterogeneous Electrocatalyst: Metal–Organic-Framework Supported Molybdenum Sulfide for Redox Mediator-Assisted Hydrogen Evolution Reaction
MoSx-SIM-NDC-SALI powder/single crystals · Single Crystal · Agilent DD2 500 MHz NMR; NDC incorporation determined by integration of pyrene linker and NDC resonances
2020 · Tuning Electrical- and Photo-Conductivity by Cation Exchange within a Redox-Active Tetrathiafulvalene-Based Metal–Organic Framework
TTF@1 crystals · Single Crystal · Framework decomposed by D2SO4 because MOF is insoluble.
2020 · Two-Dimensional Conductive Metal-Organic Frameworks Based on Truxene
2,3,7,8,12,13-hexahydroxyl truxene linker · Powder · NMR in DMSO; HRMS MALDI-TOF; liquid UV/Vis on Shimadzu UV-2600; TGA comparison.
2019 · A Li+ conductive metal organic framework electrolyte boosts the high-temperature performance of dendrite-free lithium batteries
Optimised ILE@MOF ionogel, 1.5 g ILE per 1.0 g MOF · Thin Film · Spectra of ILE and ILE@MOF recorded without spinning; Bruker AV 300.
2019 · A two-dimensional semiconducting covalent organic framework with nickel(II) coordination for high capacitive performance
Ni0-COF powder · Powder · Control framework characterisation in SI figures S3-S16 and Table S2.
2019 · A two-dimensional semiconducting covalent organic framework with nickel(II) coordination for high capacitive performance
Ni-COF black powder · Powder · Spectroscopy used to confirm C=N formation, C-O shift and Ni coordination; XPS survey and high-resolution Ni 2p.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · REDOR experiments at 293 and 223 K, 10 kHz spinning, used to probe interaction between adsorbed 13CO2 and framework protons.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · CO2-loaded SIFSIX-3-Zn measured at 9.4 T, 15 kHz MAS, contact times of 1, 4, and 9 ms.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · 19F MAS and 1H to 29Si CP/MAS spectra collected at 9.4 T for as-made, activated, and CO2-loaded SIFSIX-3-Zn; table includes all three samples.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
Activated SIFSIX-3-Zn · Powder · 67Zn experiments at 21.1 T, nu0(67Zn) = 56.3 MHz, modified quadrupolar echo pulse sequence.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
As-made SIFSIX-3-Zn · Powder · 67Zn experiments at 21.1 T, nu0(67Zn) = 56.3 MHz, modified quadrupolar echo pulse sequence, referenced to 1.0 M aqueous Zn(NO3)2.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · 67Zn wideline spectrum of CO2-loaded SIFSIX-3-Zn recorded under static conditions at 21.1 T; EFG tensor parameters extracted by simulation.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · Simulated static 13C spectra for CO2 in SIFSIX-3-Zn using a C3 wobbling rotation with motional angle of 10 deg and rates from 10^1 to 10^7 Hz.
2019 · CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy
13CO2-loaded SIFSIX-3-Zn · Powder · Static VT 13C SSNMR from 153 to 393 K at 9.4 T; DEPTH-echo pulse sequence; temperature calibration by 207Pb chemical shift of Pb(NO3)2 with +/-2 K error.
2019 · Efficient MOF-Sensitized Solar Cells Featuring Solvothermally Grown [100]-Oriented Pillared Porphyrin Framework-11 Films on ZnO/FTO Surfaces
[100]-oriented PPF-11 film on TCPP-coated ZnO-FTO · Electrode · 300 MHz; one drop CF3CO2D in DMSO-d6; compares scraped film and bulk crystals
2019 · Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film
Bulk UU-100(Co) powder · Powder · Digested MOF NMR in DCl/DMSO-d6; ATR-IR room temperature; TGA heating experiment.
2019 · Li + Ion-Conducting Sulfonate-Based Neutral Metal-Organic Framework
LiClO4-treated Cu(I)-sulfonate MOF pellet · Pellet · 500 MHz 1H NMR; 1 drop CF3CO2D in 1 mL DMSO-d6; compared digested pristine and LiClO4-treated MOF.
2019 · Photodimerization of a 1D Ladder Polymer through Single-Crystal to Single-Crystal Transformation Has an Effect on Electrical Conductivity
Compound 1 colourless block crystals · Single Crystal · As-synthesised compound 1 characterised by elemental analysis, IR, and solution 1H NMR.
2019 · Photodimerization of a 1D Ladder Polymer through Single-Crystal to Single-Crystal Transformation Has an Effect on Electrical Conductivity
Compound 2 light yellow photodimerised block crystals · Single Crystal · UV-photodimerised compound 2 characterised by elemental analysis, IR, and solution 1H NMR.
2019 · Self-assembly and optoelectronic properties of isoreticular MOF nanocrystals
off-white crystalline IRMOF-8 microstructure powder · Powder · Dry microstructure sample dissolved in d6-DMSO.
2018 · Development of a UiO-Type Thin Film Electrocatalysis Platform with Redox-Active Linkers
Zr(dcphOH-NDI) bulk microcrystalline powder · Powder · ATR-FTIR 4000-450 cm^-1; MOF digested with 25 uL HF in DMSO-d6 for NMR; TGA in air from 25 to 800 deg C at 5 deg C/min after drying.
2018 · High Proton Mobility with High Directionality in Isolated Channels of MOF-74
pH 11 NH4OH-treated Co-MOF-74 crystals before electrode configuration · Single Crystal · Co-MOF-74 crystals after pH 11 treatment, compared with as-synthesised Co-MOF-74.
2018 · High Proton Mobility with High Directionality in Isolated Channels of MOF-74
pH 3 H2SO4-treated Co-MOF-74 crystals before electrode configuration · Single Crystal · Co-MOF-74 crystals after pH 3 treatment, compared with as-synthesised Co-MOF-74.
2018 · High Proton Mobility with High Directionality in Isolated Channels of MOF-74
pH 5 H2SO4-treated Co-MOF-74 crystals before electrode configuration · Single Crystal · Co-MOF-74 crystals after pH 5 treatment, compared with as-synthesised Co-MOF-74.
2018 · High Proton Mobility with High Directionality in Isolated Channels of MOF-74
pH 7 H2O-coordinating Co-MOF-74 crystals before electrode configuration · Single Crystal · Co-MOF-74 crystals after pH 7 treatment, compared with as-synthesised Co-MOF-74.
2018 · High Proton Mobility with High Directionality in Isolated Channels of MOF-74
pH 9 NH4OH-treated Co-MOF-74 crystals before electrode configuration · Single Crystal · Co-MOF-74 crystals after pH 9 treatment, compared with as-synthesised Co-MOF-74.
2018 · Highly Conductive 2D Metal-Organic Framework Thin Film Fabricated by Liquid-Liquid Interfacial Reaction Using One-Pot-Synthesized Benzenehexathiol
BHT yellow solid · Powder · 1H NMR at 400 MHz in CD3CN; ESI-MS with BHT dissolved in dichloromethane.
2018 · Selective reduction of CO2 by conductive MOF nanosheets as an efficient co-catalyst under visible light illumination
Ni3(HITP)2 nanosheet/[Ru(bpy)3]Cl2.6H2O photocatalytic mixture · Unknown · 2 mg Ni3(HITP)2, 80 mg [Ru(bpy)3]Cl2.6H2O, 16 mL MeCN/H2O/TEOA 10:2:4 v/v/v, 80 kPa CO2, 4 C, 100 W LED at 420 nm, 7.5 cm illumination distance; gases analysed hourly by GC-TCD/FID.
2017 · Lowering Band Gap of an Electroactive Metal-Organic Framework via Complementary Guest Intercalation
Activated DSNDI-based MOF-74 powder · Powder · DSNDI-based MOF-74 spectra compared with DSNDI ligand.
2016 · Metal-organic framework nanomaterials as novel signal probes for electron transfer mediated ultrasensitive electrochemical immunoassay
as-prepared COF nanoparticles · Powder · Solid-state NMR used to confirm imine COF formation.
2015 · A porous proton-relaying metal-organic framework material that accelerates electrochemical hydrogen evolution
benzoate-modified FTO_NU-1000 · Electrode · Benzoate-modified NU-1000 sample; integration of benzoic acid and H4TBAPy linker peaks.
2015 · Confinement of single polysilane chains in coordination nanospaces
1a-PMPrS powder composite, 30 wt percent PMPrS · Powder · 29Si MAS NMR at 59.6 MHz with recycle delay of 100 s.
2015 · Confinement of single polysilane chains in coordination nanospaces
1a-PMPrS powder composite, 30 wt percent PMPrS · Powder · PMLG HETCOR spectra with contact times of 2 and 8 ms; 600 MHz 1H DQ CRAMPS at 13.6 kHz spinning.
2015 · Confinement of single polysilane chains in coordination nanospaces
1a-PMPrS powder composite, 30 wt percent PMPrS · Powder · High-resolution 1H MAS NMR at 600 MHz; MAS spinning speed 33 kHz.
2015 · Confinement of single polysilane chains in coordination nanospaces
1b-PMPrS powder composite, 30 wt percent PMPrS · Powder · 29Si MAS NMR at 59.6 MHz with recycle delay of 100 s.
2015 · Confinement of single polysilane chains in coordination nanospaces
1b-PMPrS powder composite, 30 wt percent PMPrS · Powder · PMLG HETCOR spectra of 1b-PMPrS with contact times of 5 and 8 ms as shown in SI.
2015 · Confinement of single polysilane chains in coordination nanospaces
1b-PMPrS powder composite, 30 wt percent PMPrS · Powder · High-resolution 1H MAS NMR at 600 MHz; MAS spinning speed 33 kHz.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT-bulk · Unknown · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; NaF external standard.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT@Z100 · Pellet · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; NaF external standard.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT@Z75 · Pellet · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; SI Figure S4 reports ELT@Z75 spectra at labelled temperatures.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT-bulk · Unknown · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; LiCl aqueous solution external standard.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT@Z100 · Pellet · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; LiCl aqueous solution external standard.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT@Z75 · Pellet · Hermetically sealed glass tubes; samples cooled to 123 K and heated stepwise; SI Figure S5 reports ELT@Z75 spectra at labelled temperatures.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT-bulk · Unknown · 7Li at 155.5 MHz using Bruker Diff 50 probe; hermetically sealed glass tubes; stimulated-echo pulse sequence; g = 0 to 2500 G cm^-1, Delta = 40 ms, delta = 1 ms.
2015 · Lithium Ion Diffusion in a Metal-Organic Framework Mediated by an Ionic Liquid
ELT@Z100 · Pellet · 7Li at 155.5 MHz using Bruker Diff 50 probe; hermetically sealed glass tubes; stimulated-echo pulse sequence; g = 0 to 2500 G cm^-1, Delta = 40 ms, delta = 1 ms.
2014 · Design and synthesis of hydroxide ion-conductive metal-organic frameworks based on salt inclusion
NBu4-ZIF-8 powder · Powder · NBu4-ZIF-8 dissolved in D2O/D2SO4 (9/1) with DSS internal standard; room temperature.
2014 · Immobilization of N-(3-aminopropyl)-imidazole through MOFs in proton conductive membrane for elevated temperature anhydrous applications
6% encapsulated MOFs membrane · Thin Film · Spectra of SPPO, MOFs-membrane and MOFs-NAPI-membrane
2012 · Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method
MET-6 (Zn) microcrystalline powder · Powder · Bruker DSX-300; 75.47 MHz 13C; 4 mm zirconia rotors; MAS 10 kHz; chemical shifts referenced to TMS using adamantane.
2011 · Synthesis and characterization of a novel kind soluble, conjugated, and fluorescent chelate polymer containing fluorene ring in the backbone: Optical, electrical, and electrochemical properties
poly(3,4-HBA-Cr-FDA) bulk chelate polymer · Powder · DMSO-d6 at 25 deg C; 1H at 400 MHz and 13C at 100.6 MHz; TMS internal standard.
2009 · Semiconducting neutral microstructures fabricated by coordinative self-assembly of intramolecular charge-transfer tetrathiafulvalene derivatives
compound 1 plus Pb2+ or Zn2+ solution binding samples · Model · Solution UV/Vis Job plots and spectra plus 1H NMR titrations of compound 1 with Pb(ClO4)2 or Zn(ClO4)2; addition of metal salt changed colour from yellow to deep purple.
2009 · Semiconducting neutral microstructures fabricated by coordinative self-assembly of intramolecular charge-transfer tetrathiafulvalene derivatives
compound 3 plus Pb2+ micro-nest-like structures · Powder · Pb2+ binding to triple-bond compound 3 was compared with compound 1; micro-nest-like structures were observed instead of microwires.
2009 · Soluble semi-conductive chelate polymers containing Cr(III) in the backbone: Synthesis, characterization, optical, electrochemical, and electrical properties
P-2 as-synthesised polymer · Powder · DMSO-d6 at 25 C; 400 MHz 1H and 100.6 MHz 13C, TMS internal standard
2009 · Soluble semi-conductive chelate polymers containing Cr(III) in the backbone: Synthesis, characterization, optical, electrochemical, and electrical properties
P-3 as-synthesised polymer · Powder · DMSO-d6 at 25 C; 400 MHz 1H and 100.6 MHz 13C, TMS internal standard
2008 · Synthesis and changes of conductivities and thermal stabilities of 4,4′-oxybis [N-(3,4-dihydroxybenzilidene) aniline] chelate polymers
3,4-HBA monomer, pristine pressed pellet/solid · Pellet · DMSO-d6 solvent, 25 °C, tetramethylsilane internal standard.
2008 · Synthesis and changes of conductivities and thermal stabilities of 4,4′-oxybis [N-(3,4-dihydroxybenzilidene) aniline] chelate polymers
P-3,4-HBA-Cr pristine coordination-polymer solid/pellet · Pellet · DMSO-d6/DMSO solution, 25 °C; P-3,4-HBA-Cr was relatively soluble.
1998 · Solid state electrical conductivity studies on manganese-molybdenum Schiff base polymer
dark yellow manganese-molybdenum Schiff base polymer solid · Powder · 1H NMR spectrum of coordination polymer
No mapped measurement matches these filters.
These are the exact source-preserving method strings consolidated by this technique group.
| Raw method label | Mapped measurements |
|---|---|
| Quantitative 1H NMR and TGA purity analysis | 6 |
| 7Li solid-state MAS NMR inversion-recovery T1 | 5 |
| 1H NMR and powder X-ray diffraction (PXRD) | 5 |
| 1H and 19F quantitative NMR | 4 |
| 1H PFG-NMR self-diffusion, unidirectional model | 4 |
| 1H and 13C NMR spectroscopy | 3 |
| Solid-state static 19F NMR at 376.5 MHz | 3 |
| Solid-state static 7Li NMR at 155.5 MHz | 3 |
| FT-IR, Raman, solid-state 13C NMR, XPS/EXAFS | 3 |
| variable-temperature static 7Li NMR | 3 |
| 7Li PFG-NMR self-diffusion, unidirectional model | 3 |
| cation transference number estimated from PFG-NMR diffusion constants | 3 |
| Static 67Zn SSNMR with spectral simulation | 3 |
| solid-state 13C NMR spectroscopy | 2 |
| Elemental analysis, FT-IR in KBr, and 1H NMR in d6-DMSO at 300 MHz and 298 K | 2 |
| 7Li pulsed-field gradient NMR (PFG-NMR) diffusion measurement | 2 |
| 1H NMR after acid digestion | 2 |
| Fully relaxed 29Si MAS NMR | 2 |
| 1H MAS NMR | 2 |
| CO2 electroreduction in gas-tight two-compartment H-cell; GC/NMR product analysis | 2 |
| 1H and 13C NMR spectroscopy, Bruker AC FT-NMR at 400 and 100.6 MHz | 2 |
| Digestion followed by 1H NMR guest-loading quantification | 2 |
| Elemental analysis, 1H NMR, FT-IR and UV-vis spectroscopy | 2 |
| Bulk electrolysis / chronoamperometry with NMR product quantification | 2 |
| Digestive 1H NMR spectroscopy | 1 |
| Visible-light photocatalytic CO2 reduction with online gas chromatography and 1H NMR liquid-product analysis | 1 |
| 13C NMR, MALDI-TOF MS, FTIR | 1 |
| solution-state 1H NMR after acidic digestion | 1 |
| 1H NMR and ESI-MS | 1 |
| FT-IR, 1H NMR digestion/suspension, XPS, UV-Vis-NIR DRS, EPR, and TGA | 1 |
| Acid-digested 1H NMR and CHN elemental analysis | 1 |
| 1H NMR and liquid UV-vis comparison | 1 |
| FT-IR and solid-state 13C NMR | 1 |
| FTIR, EELS, solid-state 13C CP/MAS NMR, XPS, Co K-edge XANES/EXAFS, wavelet transform, UV-vis, UPS | 1 |
| 1H NMR of digested MOF samples | 1 |
| Solid-state 13C NMR and FT-IR spectroscopy | 1 |
| 1H NMR of D2SO4-digested MOF in d6-DMSO. | 1 |
| 1H NMR isotope labelling with 14NO3- and 15NO3- | 1 |
| 1H NMR, 13C ssNMR and mass spectrometry after reduction/CO2 exposure | 1 |
| solid-state 13C NMR | 1 |
| 1H NMR, AV III 400 NMR spectrometer, DMSO-d6 | 1 |
| Quantitative 1H NMR | 1 |
| 1H NMR, 13C NMR, HRMS, UV-vis-NIR, and TGA control characterisation | 1 |
| PXRD, FT-IR, solid-state 13C NMR, XPS, SEM/TEM | 1 |
| FT-IR, solid-state 13C CP/MAS NMR, and XPS | 1 |
| 13C CP-MAS solid-state NMR with TPPM 1H decoupling | 1 |
| 1H NMR of digested MOF, ATR-IR, and TGA | 1 |
| 1H NMR of digested CDL-MOF1 | 1 |
| catalytic cyanosilylation; conversion by 1H NMR | 1 |
| 1H and 11B NMR hidden-boron catalysis controls | 1 |
| hydroboration condition optimisation by 1H NMR conversion | 1 |
| catalytic hydroboration; conversion/yield by 1H NMR | 1 |
| 2D 1H-13C and 1H-29Si HETCOR NMR; 2D 1H-1H DQ CRAMPS | 1 |
| 2D 1H-13C and 1H-29Si HETCOR NMR | 1 |
| 1H NMR of digested MOF | 1 |
| FTIR-ATR, 1H NMR after HF digestion, and TGA | 1 |
| Solution-phase 1H NMR spectroscopy | 1 |
| elemental analysis, 1H NMR, 13C NMR, ESI-MS and ATR-IR | 1 |
| 1H NMR spectroscopy in d-DMSO | 1 |
| 1H NMR (Agilent-400 MR DD 2) in d6-DMSO | 1 |
| NMR isotope labelling | 1 |
| Potentiostatic nitrate electroreduction with UV-vis/NMR product quantification | 1 |
| Solution UV/Vis and 1H NMR binding analysis of compound 1 with Pb(ClO4)2 and Zn(ClO4)2 | 1 |
| UV/Vis and NMR spectra plus morphology comparison | 1 |
| 1H NMR digestion | 1 |
| 1H NMR after digestion | 1 |
| CO2 electroreduction in H-type cell with GC/NMR product analysis | 1 |
| Faradaic efficiency and CH4 partial current density from GC/NMR | 1 |
| 1H NMR, FTIR, XPS, UV-Vis absorption | 1 |
| 119Sn solid-state MAS NMR | 1 |
| normalised 7Li NMR line-width comparison | 1 |
| 1H NMR spectroscopy of digested MOF samples | 1 |
| 1H NMR of digested CAU-24 in D2SO4/DMSO-d6 | 1 |
| 1H NMR spectroscopy, Hitachi R-600 high resolution spectrometer | 1 |
| 1H NMR spectroscopy | 1 |
| 13C{1H} REDOR SSNMR | 1 |
| 19F to 13C CP/MAS SSNMR | 1 |
| 19F MAS and 1H to 29Si CP/MAS SSNMR | 1 |
| Motional simulation of static 13C SSNMR spectra | 1 |
| Variable-temperature static 13C SSNMR with analytical and motional simulations | 1 |
| digested-sample 1H NMR integration | 1 |
| 1H NMR in CDCl3 | 1 |
| 1H and 13C NMR spectroscopy using Bruker AC FT-NMR | 1 |
| CO2 electroreduction in H-type cell with LSV, chronoamperometry, GC, and 1H NMR product analysis | 1 |
| Solid-state 27Al MAS NMR | 1 |
| Solid-state 7Li NMR | 1 |
| Isotopically labelled nitrogen reduction reaction with UV-vis and 1H NMR product quantification | 1 |
| Chronoamperometry urea electrosynthesis with diacetyl monoxime, indophenol blue, NMR and GC analysis | 1 |
| 1H NMR | 1 |
| Ni K-edge XANES/EXAFS, XPS, solid-state 13C NMR and FT-IR | 1 |
| HPLC-MS and 1H NMR of AA oxidation products | 1 |
| Long-duration electrolysis with NMR product quantification | 1 |