Measurement evidence
Design and synthesis of hydroxide ion-conductive metal-organic frameworks based on salt inclusion · Sadakiyo M., Kasai H., Kato K. et al. · Journal of the American Chemical Society · 2014 · 1702-1705
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
NBu4-ZIF-8 powder · Powder
Room-temperature infrared spectra compared ZIF-8 and NBu4-ZIF-8.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Butyl-group CH stretching mode | 2876 cm-1 | — | — | Text Exact Reported | 1703 · Characterisation · Figure S1 |
| Butyl-group CH stretching mode | 2961 cm-1 | — | — | Text Exact Reported | 1703 · Characterisation · Figure S1 |
NBu4-ZIF-8 powder · Powder
NBu4-ZIF-8 dissolved in D2O/D2SO4 (9/1) with DSS internal standard; room temperature.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| NBu4+ 1H NMR resonances | delta = 3.18, 1.64, 1.37, and 0.95 ppm | — | — | Text Exact Reported | S3 · Physical measurements · Figure S2 |
| No detectable NHBu3+ signals | No signals assignable to NHBu3+ were recognised | — | — | Text Qualitative | 1703 · Characterisation · Figure S2 |