Other — Design and synthesis of hydroxide ion-conductive metal-organic frameworks based on salt inclusion

Measurement evidence

Other

Design and synthesis of hydroxide ion-conductive metal-organic frameworks based on salt inclusion · Sadakiyo M., Kasai H., Kato K. et al. · Journal of the American Chemical Society · 2014 · 1702-1705

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetry analysis

NBu4-ZIF-8 powder · Powder

Nitrogen flow 100 ml/min; heating rate 5 C/min; RT to 900 C.

Atmosphere
N2
Context
Salt-loaded sample compared with pristine ZIF-8.
Measurement source
S3 · Physical measurements · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Salt inclusion state stabilitystable up to 120 CText
Rounded Reported
1703 · Thermal analysis · Figures S3-S4
NBu4-ZIF-8 weight-loss event temperatureweight loss at 127 CText
Exact Reported
1703 · Thermal analysis · Figure S3

Temperature-programmed desorption mass spectrometry

NBu4-ZIF-8 powder · Powder

Helium flow 30 ml/min; heating rate 3 C/min.

Atmosphere
He
Context
Salt-loaded sample.
Measurement source
S3 · Physical measurements · Figure S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TPD-MS desorbed species mass 18M = 18 (H2O)Caption
Exact Reported
S5 · Figure S4 · Figure S4
TPD-MS desorbed species mass 44M = 44 (CO2)Caption
Exact Reported
S5 · Figure S4 · Figure S4
TPD-MS desorbed species mass 56M = 56 (C4H8)Caption
Exact Reported
S5 · Figure S4 · Figure S4