FT-IR, Raman, solid-state 13C NMR, XPS/EXAFS
Infrared spectroscopyRaman spectroscopyX-ray photoelectron spectroscopyX-ray absorption spectroscopyNuclear magnetic resonance
as-prepared SJTU-201 powder · Powder
coordination-bond confirmation for Rh-isocyano MOFs
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| EXAFS Rh-C first-shell scattering peak | 1.50 A | — | — | Text Exact Reported | 2 · Design and Synthesis · Figure S33 |
| coordinated isocyano FT-IR peak | 2140 cm-1 | — | — | Text Exact Reported | 2 · Design and Synthesis · Figures S20-S22 |
| coordinated isocyano Raman peak | 2184 cm-1 | — | — | Caption Exact Reported | 37-39 · Supplementary Figures · Figures S23-S25 |
| 13C SSNMR Rh-CN signal | 147.69 ppm | — | — | Text Exact Reported | 2 · Design and Synthesis · Figures S26-S28 |