Diffraction Structure — 2D Rhodium-Isocyanide Frameworks

4 measurement groups · 20 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

as-prepared SJTU-201 powder · Powder

as-prepared powder; Cu Kalpha1 PXRD; refined lattice parameters reported

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
interlayer spacing	3.47 A	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
refined lattice parameters	a=b=11.3 A; c=3.56 A; alpha=beta=81 deg; gamma=90 deg	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
adjacent-layer Rh-Rh distance	about 3.56 A	—	—	Caption Rounded Reported	4 · Crystalline Structures · Figure 2
Pawley Rp	5.71%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
Pawley Rwp	5.95%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
layer stacking assignment	inclined AA	—	—	Text Qualitative	5 · Crystalline Structures · Figure 2

as-prepared SJTU-202 powder · Powder

as-prepared powder; Cu Kalpha1 PXRD; refined lattice parameters reported

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
interlayer spacing	3.55 A	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
refined lattice parameters	a=b=15.8 A; c=3.55 A; alpha=beta=gamma=90 deg	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
adjacent-layer Rh-Rh distance	about 3.55 A	—	—	Caption Rounded Reported	4 · Crystalline Structures · Figure 2
Pawley Rp	2.97%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
Pawley Rwp	3.22%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
layer stacking assignment	eclipsed AA	—	—	Text Qualitative	5 · Crystalline Structures · Figure 2

as-prepared SJTU-203 powder · Powder

as-prepared powder; Cu Kalpha1 PXRD; refined lattice parameters reported

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
interlayer spacing	3.27 A	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
refined lattice parameters	a=b=17.9 A; c=3.59 A; alpha=beta=74 deg; gamma=90 deg	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
adjacent-layer Rh-Rh distance	about 3.59 A	—	—	Caption Rounded Reported	4 · Crystalline Structures · Figure 2
Pawley Rp	6.68%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
Pawley Rwp	5.14%	—	—	Text Exact Reported	5 · Crystalline Structures · Figure 2
layer stacking assignment	inclined AA	—	—	Text Qualitative	5 · Crystalline Structures · Figure 2

as-prepared SJTU-202 powder · Powder

H2O, HCl, NaOH, air exposure, and TGA stability checks

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
air stability duration	30 days exposure to air	—	—	Text Exact Reported	5 · Crystalline Structures · Figure S39
thermal stability threshold for SJTUs	stable up to 300 C with less than 10% weight loss	—	—	Text Rounded Reported	5 · Crystalline Structures · Figure S40