Spectroscopy — Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film

Measurement evidence

Spectroscopy

Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film · Roy S., Huang Z., Bhunia A. et al. · Journal of the American Chemical Society · 2019 · 15942-15950

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

1H NMR of digested MOF, ATR-IR, and TGA

Bulk UU-100(Co) powder · Powder

Digested MOF NMR in DCl/DMSO-d6; ATR-IR room temperature; TGA heating experiment.

Temperature
293 for NMR
Context
pristine framework powder
Measurement source
15944 · Synthesis and Characterization · Figures S12-S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Trapped DMF per cobaloxime linker~3 DMF per cobaloxime linkerapproximatelyCaption
Approximate
S15 · Figure caption · Figure S13
Zr-mu3-O ATR-IR stretch659 cm-1Text
Exact Reported
15943 · Synthesis and Characterization · Figure S12
Initial guest-solvent loss temperature regionbelow 100 CbelowText
Approximate
15944 · Synthesis and Characterization · Figure S14