cMOF Evidence Base
Microscopy Morphology — Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film

Measurement evidence

Microscopy Morphology

Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film · Roy S., Huang Z., Bhunia A. et al. · Journal of the American Chemical Society · 2019 · 15942-15950

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM, SEM-EDX mapping, and ICP-OES

Scanning electron microscopyElemental microanalysis and mappingBulk elemental and compositional analysis

Bulk UU-100(Co) powder · Powder

SEM/EDX on rod-shaped UU-100(Co) crystallites; ICP-OES after acid/peroxide microwave digestion.

Context
pristine framework powder
Measurement source
15943 · Synthesis and Characterization · Figure 2B; Figures S8-S9; Table S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM rod crystallite length~1-3 um—range 1-3 umText
Range		15943 · Synthesis and Characterization · Figure 2B
SEM-EDX Zr:Co ratio2.4 +/- 0.3—+/- 0.3Text
Exact Reported		15943 · Synthesis and Characterization · Figures 2B and S8; Table S2
ICP-OES Zr:Co ratioMarked as a best value within this paper2.8 +/- 0.3—+/- 0.3Text
Exact Reported		15943 · Synthesis and Characterization