Measurement evidence
Metal-Organic Framework Assembled on Oriented Nanofiber Arrays for Field-Effect Transistor and Gas Sensor-Based Applications · Mu J., Zhong X., Dai W. et al. · Molecules · 2022 · 2131
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Cu3(HITP)2 NFAs on PDMS-PCDA/Cu, 500 r/min · Electrode
PDMS-PCDA/Cu and PDMS-PCDA/Cu3(HITP)2 compared.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu3(HITP)2 NFA FTIR characteristic peak | 1144 cm-1 | — | — | Text Exact Reported | 6 · Results and Discussion · Figure 3a |
oriented PDMS-PCDA/Cu NFAs · Thin Film
PDMS, PCDA and PDMS-PCDA compared.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PDMS-PCDA amide II FTIR peak | 1536 cm-1 | — | — | Text Exact Reported | 5 · Results and Discussion · Figure 2a |
| PDMS Si-NH2 FTIR peak | 3423 cm-1 | — | — | Text Exact Reported | 5 · Results and Discussion · Figure 2a |
oriented PDMS-PCDA/Cu NFAs · Thin Film
PDMS-PCDA ligand characterised in CDCl3; solvent signals used as internal standards.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PDMS-PCDA 13C NMR carbonyl resonance | delta 163.57 | — | — | Text Exact Reported | S3 · Section S2. Chemical Synthesis · Figure S1 |
| PDMS-PCDA 1H NMR aromatic doublet | delta 8.36 (d, J = 8.0 Hz, 2H) | — | — | Text Exact Reported | S3 · Section S2. Chemical Synthesis · Figure S1 |
Cu3(HITP)2 NFAs on PDMS-PCDA/Cu, 500 r/min · Electrode
Survey and high-resolution C1s, N1s and Cu2p spectra for PDMS-PCDA/Cu3(HITP)2 NFAs.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu 2p3/2 lower binding-energy component | 952.79 eV | — | — | Text Exact Reported | 6 · Results and Discussion · Figure 3b |
| Residual NH4/unreacted precursor assessment | No additional NH4+ cations and no residual unreacted precursors/solvents indicated by N1s XPS | — | — | Text Qualitative | 6 · Results and Discussion · Figure 3b |
oriented PDMS-PCDA/Cu NFAs · Thin Film
Survey and high-resolution C1s, N1s and Cu2p spectra.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| C1s C=O binding energy | 286.48 eV | — | — | Text Exact Reported | 5 · Results and Discussion · Figure 2b |
| Cu 2p3/2 binding energy in PDMS-PCDA/Cu | 932.41 eV | — | — | Text Exact Reported | 5-6 · Results and Discussion · Figure 2b |