Microscopy Morphology — Metal-Organic Framework Assembled on Oriented Nanofiber Arrays for Field-Effect Transistor and Gas Sensor-Based Applications

Measurement evidence

Microscopy Morphology

Metal-Organic Framework Assembled on Oriented Nanofiber Arrays for Field-Effect Transistor and Gas Sensor-Based Applications · Mu J., Zhong X., Dai W. et al. · Molecules · 2022 · 2131

4 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

optical photography and SEM/EDX mapping

oriented PDMS-PCDA/Cu NFAs · Thin Film

PDMS-PCDA/Cu fibre arrays on 1 cm x 1 cm (n++) Si after electrostatic spinning.

Context
Template precursor morphology.
Measurement source
5-6 · Results and Discussion · Figure 2c-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PDMS-PCDA/Cu fibre morphologyuniform thickness, good aspect ratio, smooth surface; C, N and Cu uniformly distributedText
Qualitative
6 · Results and Discussion · Figure 2d

SEM and EDS elemental mapping

Cu3(HITP)2 NFA chemiresistor sensor · Electrode

Cu3(HITP)2 fibre membrane SEM image and C/N/Cu elemental maps.

Context
Composite Cu3(HITP)2 fibre membrane characterisation.
Measurement source
S6 · Section S3. Characterization · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu3(HITP)2 fibre membrane elemental mappingC, N and Cu elemental maps shown for the Cu3(HITP)2 fibre membraneCaption
Qualitative
S6 · Section S3. Characterization · Figure S3

SEM imaging of FET electrode/fibre arrays

Cu3(HITP)2 NFAs on PDMS-PCDA/Cu, 500 r/min · Electrode

SEM images of Au electrode evaporated on Cu3(HITP)2 NFAs of 300, 400 and 500 r/min and corresponding interelectrode fibre arrays.

Geometry
Au electrode on Cu3(HITP)2 NFA-based FET.
Context
Composite NFA FET morphology.
Measurement source
S7 · Section S3. Characterization · Figure S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM coverage of 300/400/500 r/min FET samplesSEM images reported for Au electrodes on Cu3(HITP)2 NFAs prepared at 300, 400 and 500 r/minCaption
Qualitative
S7 · Section S3. Characterization · Figure S4

TEM, HR-TEM and FFT

Cu3(HITP)2 NFAs on PDMS-PCDA/Cu, 500 r/min · Electrode

Interface and lattice observation of PDMS-PCDA/Cu3(HITP)2 NFAs.

Context
Composite conductive-MOF NFA structure.
Measurement source
8 · Results and Discussion · Figure 4c-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Black interface width at fibre edgeabout 50 nmaboutText
Approximate
8 · Results and Discussion · Figure 4c
Cu3(HITP)2 crystal-plane spacing1.9 nmText
Exact Reported
8 · Results and Discussion · Figure 4d