Spectroscopy — Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method

Measurement evidence

Spectroscopy

Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method · Gandara F., Uribe-Romo F.J., Britt D.K. et al. · Chemistry - A European Journal · 2012 · 10595-10601

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

13C CP-MAS solid-state NMR with TPPM 1H decoupling

Nuclear magnetic resonance

MET-6 (Zn) microcrystalline powder · Powder

Bruker DSX-300; 75.47 MHz 13C; 4 mm zirconia rotors; MAS 10 kHz; chemical shifts referenced to TMS using adamantane.

Temperature: ambient
Atmosphere: ambient pressure
Geometry: solid-state MAS rotor
Context: pristine MET-6 framework powder
Measurement source: SI p.6 · Section S2 · Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
free triazole carbon resonance comparison	130.3 ppm in triazole	—	—	Text Exact Reported	p.2, article p.10596 · Results and Discussion · Figure S1
13C CP-MAS triazolate carbon resonance	128.8 ppm	—	—	Text Exact Reported	p.2, article p.10596 · Results and Discussion · Figure S1