Other — Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method

Measurement evidence

Other

Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method · Gandara F., Uribe-Romo F.J., Britt D.K. et al. · Chemistry - A European Journal · 2012 · 10595-10601

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SQUID magnetic susceptibility

MET-2 (Mn) microcrystalline powder · Powder

Quantum Design MPMS; 4.6 mg MET-2 in diamagnetic polycarbonate capsule; 1 kOe field; 5-300 K, cooling then warming.

Temperature
5-300
Atmosphere
sealed capsule
Geometry
powder in capsule
Context
pristine MET-2 framework powder
Measurement source
SI p.21 · Section S6 · Figures S18-S19
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Curie-Weiss temperature-21.9 KText
Exact Reported
p.4, article p.10598 · Magnetic susceptibility · Figures S18-S19
calculated effective magnetic momentcalcd. mu_eff = 5.8 mu_BText
Exact Reported
p.4, article p.10598 · Magnetic susceptibility · Figures S18-S19
Mn spin-state assignmentMn atoms are in high spinText
Qualitative
p.4, article p.10598 · Magnetic susceptibility · Figures S18-S19

Thermogravimetric analysis

MET-5 (Cu) microcrystalline powder · Powder

TA Instruments Q-500; platinum pans; continuous nitrogen flow; 5 C/min heating rate.

Temperature
variable heating
Atmosphere
continuous-flow nitrogen
Geometry
powder in platinum pan
Context
pristine MET powders
Measurement source
SI pp.18-20 · Section S5 · Figures S12-S17
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
decomposition-temperature rangeapproximately 250 C in MET-5 to 400 C in MET-2Text
Range
p.4, article p.10598 · Thermal stability · Figures S12-S17
thermal stability before decompositionno weight loss below decomposition temperatureText
Qualitative
p.4, article p.10598 · Thermal stability · Figures S12-S17