Microscopy Morphology — Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method

Measurement evidence

Microscopy Morphology

Porous, conductive metal-triazolates and their structural elucidation by the charge-flipping method · Gandara F., Uribe-Romo F.J., Britt D.K. et al. · Chemistry - A European Journal · 2012 · 10595-10601

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Scanning electron microscopy

MET-6 (Zn) microcrystalline powder · Powder

MET-2 and MET-6 powders dispersed on sticky carbon, gold coated at 70 mTorr Ar for 30 s, 15 mA; JEOL JSM-6700, SEI/LEI, 7 kV.

Temperature
ambient
Atmosphere
argon during sputter coating
Geometry
powder on flat aluminium holder
Context
pristine framework powder
Measurement source
SI p.16 · Section S4 · Figures S10-S11
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM particle morphologyclusters of octahedral particles about 1 x 1 micrometreText
Approximate
SI p.16 · Section S4 · Figures S10-S11

Scanning electron microscopy of conductivity pellet

MET-3 freshly prepared pressed pellet · Pellet

SEM image of MET-3 pellet used for conductivity measurements; figure caption reports 30000x.

Geometry
pressed pellet morphology
Context
pristine MET-3 framework pellet
Measurement source
p.5, article p.10599 · Electrical conductivity · Figure 6c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
grain-boundary limitationlarge number of grain boundaries observed in SEM pellet imageText
Qualitative
p.5, article p.10599 · Electrical conductivity · Figure 6c