Measurement evidence
Two one-dimensional germanium(IV) coordination polymers based on macrocyclic tetraaza[14]annulene with notable semiconducting property · Wang X., Shen X., Zhang Y.-J. et al. · Inorganic Chemistry Communications · 2013 · 45-49
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
pressed-pellet powder compaction of compound 1 · Pellet
Bulk powder of compound 1 obtained faster by direct stirring reaction; yield reported in main-text synthesis note.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| bulk powder synthesis yield of compound 1 | 86% | 0.86 fraction | — | Text Exact Reported | 4 · Reference 31, synthesis of 1 |
pressed-pellet powder compaction of compound 1 · Pellet
TGA/DSC thermal trace in supporting information; atmosphere and ramp rate not stated.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| decomposition temperature of compound 1 | 356 deg C | 629.15 K | — | Caption Exact Reported | 3 · Supporting Information, 2. TGA/DCS trace · Fig. S3 |
| DSC event temperature for compound 1 | 371 deg C from labelled SI trace | 644.15 K | — | Figure Axis Rounded Reported | 3 · Supporting Information, TGA/DSC trace · Fig. S3 |
| DSC event temperature for compound 1 | 481 deg C from labelled SI trace | 754.15 K | — | Figure Axis Rounded Reported | 3 · Supporting Information, TGA/DSC trace · Fig. S3 |
pressed-pellet powder compaction of compound 2 · Pellet
Powder of compound 2 obtained by a method similar to compound 1; yield reported in main-text synthesis note.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| bulk powder synthesis yield of compound 2 | 83% | 0.83 fraction | — | Text Exact Reported | 4 · Reference 32, synthesis of 2 |
pressed-pellet powder compaction of compound 2 · Pellet
TGA/DSC thermal trace in supporting information; atmosphere and ramp rate not stated.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| decomposition temperature of compound 2 | 334 deg C | 607.15 K | — | Caption Exact Reported | 3 · Supporting Information, 2. TGA/DCS trace · Fig. S4 |
| DSC event temperature for compound 2 | 507 deg C from labelled SI trace | 780.15 K | — | Figure Axis Rounded Reported | 3 · Supporting Information, TGA/DSC trace · Fig. S4 |