Porosity — Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties

Measurement evidence

Porosity

Toward High-Performance Metal–Organic-Framework-Based Quasi-Solid-State Electrolytes: Tunable Structures and Electrochemical Properties · Dong P., Zhang X., Hiscox W. et al. · Advanced Materials · 2023 · 2211841

4 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 physisorption at 77 K

HKUST-1 nanoparticles · Powder

Degassed MOFs at 150 C for 12 h before measurement.

Temperature
77
Geometry
powder adsorption
Context
pristine MOF host
Measurement source
SI p.S-30 · N2 adsorption-desorption isotherms · Table S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area373 m2 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3
pore size range0.80-25.25 nmSI Table
Range
SI p.S-30 · N2 physisorption · Table S3
cumulative pore volume0.63 cm3 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3

N2 physisorption at 77 K

Mg-MOF-74 hollow nanoparticle aggregates · Powder

Degassed MOFs at 150 C for 12 h before measurement.

Temperature
77
Geometry
powder adsorption
Context
pristine MOF host
Measurement source
SI p.S-79 · N2 adsorption-desorption isotherms · Table S10
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area1623 m2 g-1SI Table
Exact Reported
SI p.S-79 · N2 physisorption · Table S10
pore size range0.86-27.27 nmSI Table
Range
SI p.S-79 · N2 physisorption · Table S10
cumulative pore volume0.65 cm3 g-1SI Table
Exact Reported
SI p.S-79 · N2 physisorption · Table S10

N2 physisorption at 77 K

MOF-5 nanoparticles · Powder

Degassed MOFs at 150 C for 12 h before measurement.

Temperature
77
Geometry
powder adsorption
Context
pristine MOF host
Measurement source
SI p.S-30 · N2 adsorption-desorption isotherms · Table S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area720 m2 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3
pore size range0.50-27.27 nmSI Table
Range
SI p.S-30 · N2 physisorption · Table S3
cumulative pore volume0.26 cm3 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3

N2 physisorption at 77 K

Zn-MOF-74 activated nanoparticles · Powder

Degassed MOFs at 150 C for 12 h before measurement.

Temperature
77
Geometry
powder adsorption
Context
pristine MOF host
Measurement source
SI p.S-30 · N2 adsorption-desorption isotherms · Table S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area882 m2 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3
pore size range0.80-27.27 nmSI Table
Range
SI p.S-30 · N2 physisorption · Table S3
cumulative pore volume0.65 cm3 g-1SI Table
Exact Reported
SI p.S-30 · N2 physisorption · Table S3