Powder X-ray diffraction, SmartLab-3 kW; simulated and experimental comparisons in SI Figure S1
Bi(HHTP) 4/8/12/20 h nanobelt powder series · Powder
As-prepared Bi(HHTP) samples; crystallite sizes calculated using the Debye-Scherrer equation.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Debye-Scherrer crystallite size range | about 26-31 nm | — | — | Text Range | p003 / article p.4828 · Structural and physicochemical characterization · Figure S2 |
| PXRD phase assignment | diffraction peaks agree well with reported Bi(HHTP) crystals | — | — | Text Qualitative | p003 / article p.4828 · Structural and physicochemical characterization · Figure S1 |
| residual bismuth acetate peak position | weak peak at 2theta = 6.74 deg | — | — | Text Rounded Reported | p003 / article p.4828 · Structural and physicochemical characterization · Figure S1 |