Other

Other

Cofacial Assembly of Metallomacrocycles as an Approach to Controlling Lattice Architecture in Low-Dimensional Molecular Solids. Chemical, Structural, Oxidation-State, Transport, and Optical Properties of the Coordination Polymer [Fe(phthalocyaninato)(μ-pyrazine)]n and the Consequences of Halogen Doping · Diel B.N., Inabe T., Jaggi N.K. et al. · Journal of the American Chemical Society · 1984 · 3207-3214

TGA/DTA

Calorimetry and thermal analysis Thermogravimetric analysis

Table IV iodine-doped TGA/DTA series · Powder

Netzsch-Simultan thermoanalyser under nitrogen, heating rate 2 deg/min; Al2O3 standard for DTA.

Atmosphere: nitrogen
Context: iodine-doped target samples
Measurement source: 3210 · TGA/DTA Measurements; Iodine Doping Process · Table IV

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TGA total mass loss found, y = 0.38	16.9%	—	—	Table Exact Reported	3210 · Iodine Doping Process · Table IV
TGA total mass loss found, y = 1.49	31.2%	—	—	Table Exact Reported	3210 · Iodine Doping Process · Table IV
TGA stage 1 iodine loss, y = 2.54	120-200 deg C; mass loss 29.6% found (33.2% calculated)	—	—	Table Exact Reported	3210 · Iodine Doping Process · Table IV
TGA stage 2 pyrazine loss, y = 2.54	235-280 deg C; mass loss 7.9% found (8.2% calculated)	—	—	Table Exact Reported	3210 · Iodine Doping Process · Table IV
TGA total mass loss found, y = 2.54	40.7%	—	—	Table Exact Reported	3210 · Iodine Doping Process · Table IV

1 measurement group · 5 results