Diffraction Structure — Two-dimensional conductive metal-organic framework with 2,3,6,7,14,15-triptycenehexathiol (TCHT) ligand: synthesis, structure, electrical conductivity and CO2RR activity

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Cu-TCHT black powder · Powder

Rigaku SmartLab Studio II; Cu Kalpha lambda 1.5405 A; 2theta range 2-50 deg; 1 deg/min and 0.02 deg/step.

Geometry: powder
Context: as-synthesised pristine Cu-TCHT
Measurement source: 25728 · Synthesis and characterization of Cu-TCHT · Fig. 4g,h

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Honeycomb model periodicity	approximately 22 A	—	—	Text Approximate	25728 · Synthesis and characterization of Cu-TCHT · Fig. 4h
PXRD broad peak 1	4.3 deg 2theta; d approximately 20 A	—	—	Text Rounded Reported	25728 · Synthesis and characterization of Cu-TCHT · Fig. 4g
PXRD broad peak 2	8.5 deg 2theta; d approximately 10 A	—	—	Text Rounded Reported	25728 · Synthesis and characterization of Cu-TCHT · Fig. 4g

HMTTC precursor · Powder

Rigaku XtaLAB AFC10; Mo Kalpha radiation; 120 K.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HMTTC crystal unit-cell volume	1474.61(12) A3	—	(12)	SI Table Exact Reported	S5 · Table S1 · Table S1

TCHT ligand powder/single crystal · Powder

Rigaku XtaLAB AFC10; HyPix-6000HE detector; Mo Kalpha lambda 0.7107 A; cryogenic equipment GN-2D/S.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TCHT crystal a axis	10.0043(8) A	—	(8)	SI Table Exact Reported	S6 · Table S2 · Table S2
TCHT crystal unit-cell volume	1147.2(2) A3	—	(2)	SI Table Exact Reported	S6 · Table S2 · Table S2