cMOF Evidence Base
Microscopy Morphology — A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls

Measurement evidence

Microscopy Morphology

A Mixed Heterobimetallic Y/Eu-MOF for the Cyanosilylation and Hydroboration of Carbonyls · Echenique-Errandonea E., Lopez-Vargas M.E., Perez J.M. et al. · Catalysts · 2022 · 299

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM-EDX mapping

Scanning electron microscopyElemental microanalysis and mapping

Y/Eu-MOF crystalline catalyst · Single Crystal

SEM Leo 1430 VP with EDX microanalysis; mapping of bulk Y/Eu-MOF material and one single crystal discussed in main text.

Context
pristine mixed-metal framework
Measurement source
S17 · 9. Scanning Electron Microscopy · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
EDX europium weight percentage21.526——SI Table
Exact Reported		S17 · 9. Scanning Electron Microscopy · Figure S3
EDX oxygen weight percentage35.707——SI Table
Exact Reported		S17 · 9. Scanning Electron Microscopy · Figure S3
Y to Eu ratio in one single crystal3.25——Text
Exact Reported		3 · 2.2 Chemical Composition
EDX yttrium weight percentage41.004——SI Table
Exact Reported		S17 · 9. Scanning Electron Microscopy · Figure S3

optical microscopy particle-size distribution

Y/Eu-MOF crystalline catalyst · Single Crystal

Catalyst suspended in distilled water, shaken vigorously, sedimented 5 min, then deposited/non-suspended and steadily suspended fractions separated; 250 particles analysed per fraction.

Context
pristine mixed-metal framework
Measurement source
S18-S20 · 10. Particle size distribution of catalyst · Figures S4-S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
deposited fraction of catalyst68% of total catalyst——Text
Exact Reported		4 · 2.3 Chemical Stability and Electrophoretic Behavior · Figure S4 referenced
deposited fraction average particle size12 +/- 6 um—+/- 6 umText
Exact Reported		4 · 2.3 Chemical Stability and Electrophoretic Behavior · Figure S4 referenced
suspended fraction of catalyst32% of total catalyst——Text
Exact Reported		8 · Supplementary Materials · Figure S5 referenced
suspended fraction average particle size8 +/- 4 um—+/- 4 umText
Exact Reported		4 · 2.3 Chemical Stability and Electrophoretic Behavior · Figure S5 referenced