Diffraction Structure — MOF Nanosheet Reconstructed Two-Dimensional Bionic Nanochannel for Protonic Field-Effect Transistors

Measurement evidence

Diffraction Structure

MOF Nanosheet Reconstructed Two-Dimensional Bionic Nanochannel for Protonic Field-Effect Transistors · Wu G.-D., Zhou H.-L., Fu Z.-H. et al. · Angewandte Chemie - International Edition · 2021 · 9931-9935

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Crystal-structure assignment from reported Cu-TCPP structure and TEM/SAED confirmation

Crystalline ultrathin Cu-TCPP nanosheets · Nanosheet

Cu-TCPP nanosheet/framework structural description

Context
pristine Cu-TCPP framework
Measurement source
2 · Main text · Figure 1a,c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Layer spacing shown in structural figure0.68 nm0.68 nmFigure Axis
Rounded Reported
2 · Figure · Figure 1a
Layered reticular Cu-TCPP structureReticular layered structure in the ab plane; neighbouring layers stack along c axis through weak interactions.Text
Qualitative
2 · Main text · Figure 1a

Grazing-incidence X-ray diffraction, in-plane and out-of-plane

Cu-TCPP thin film with 10 layer-by-layer deposition cycles · Thin Film

Cu-TCPP thin film with 10 deposition cycles; orientation compared with simulated pattern

Context
pristine oriented thin film
Measurement source
2 · Main text · Figure 2a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
In-plane GIXRD orientationIn-plane patterns only show (hk0) peaks.Text
Qualitative
2 · Main text · Figure 2a
Out-of-plane GIXRD orientationOut-of-plane patterns show an (00l) peak, assigned in figure as 002.Text
Qualitative
2 · Main text · Figure 2b

Water immersion stability test with XRD and SEM

Cu-TCPP thin film with 10 layer-by-layer deposition cycles · Thin Film

Cu-TCPP thin film immersed in water for 40 days

Atmosphere
water
Context
pristine thin film
Measurement source
2 · Main text · Figure 2d; Figure S3; Figure S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Water stability durationstable for 40 days in water40 dayText
Exact Reported
2 · Main text · Figure 2d; Figure S3; Figure S4