Diffraction Structure — Magnetic and electrical behaviors of the homo-and heterometallic 1d and 3d coordination polymers based on the partial decomposition of the [cr(C2o4)3]3− building block

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Compound 1 yellow crystals / polycrystalline pressed pellet · Pellet

single crystal; data collected at 293(2) K; structure solved with SHELXS97 and refined with SHELXL-2017

Temperature: 293(2)
Geometry: single crystal 0.23 x 0.14 x 0.09 mm
Context: pristine coordination polymer single crystal
Measurement source: 4 · 2.3. Single-Crystal X-ray Structural Study · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Space group of compound 1	C2/c	—	—	Table Exact Reported	4 · 2.3. Single-Crystal X-ray Structural Study · Table 1

Compound 2 green prismatic crystals / polycrystalline pressed pellet · Pellet

single crystal; data collected at 100(2) K; structure solved with SHELXS97 and refined with SHELXL-2017

Temperature: 100(2)
Geometry: single crystal 0.80 x 0.50 x 0.20 mm
Context: pristine coordination polymer single crystal
Measurement source: 4 · 2.3. Single-Crystal X-ray Structural Study · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Space group of compound 2	P-1	—	—	Table Exact Reported	4 · 2.3. Single-Crystal X-ray Structural Study · Table 1

Compound 3 dark green prismatic crystals / polycrystalline pressed pellet · Pellet

single crystal; data collected at 293(2) K; Friedel pairs measured to establish absolute structure

Temperature: 293(2)
Geometry: single crystal 0.25 x 0.15 x 0.05 mm
Context: pristine coordination polymer single crystal
Measurement source: 4 · 2.3. Single-Crystal X-ray Structural Study · Table 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Space group of compound 3	P41212	—	—	Table Exact Reported	4 · 2.3. Single-Crystal X-ray Structural Study · Table 1
Underlying topology of compound 3	diamondoid (dia) or (6^6) topology	—	—	Text Qualitative	9 · 3.3. Molecular and Crystal Structures of Compounds 1-3 · Figures 5-7