cMOF Evidence Base
Diffraction Structure — Bimetallic conductive MOF single crystals designed as high-performance anodes for lithium-ion batteries

Measurement evidence

Diffraction Structure

Bimetallic conductive MOF single crystals designed as high-performance anodes for lithium-ion batteries · Xu T., Li S., Mi H. et al. · Journal of Power Sources · 2026 · 240056

5 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Post-cycling XRD, TEM and SAED

X-ray diffraction and scatteringTransmission electron microscopy

CNH electrode after cycling · Electrode

CNH electrode after cycling; XRD after 600 cycles and SEM/TEM/SAED after cycling referenced in SI.

Atmosphere
room temperature
Geometry
CR2025 Li half-cell
Context
cycled target composite electrode
Measurement source
SI p.6-p.7 · Supplementary figures · Fig. S10; Fig. S11
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CNH post-cycling structural evolutionsingle-crystal diffraction spots disappeared; transformed from single crystal to amorphous state——Text
Qualitative		p.6 · Results and discussion · Fig. S11

Powder X-ray diffraction

X-ray diffraction and scattering

CNH (1:1) as-synthesised powder · Powder

Supplementary XRD patterns of CNH(3:1), CNH and CNH(1:1); rendered SI page read visually.

Context
ratio-variant pristine framework
Measurement source
SI p.2 · Supplementary figures · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co/Ni-ratio XRD qualitative comparisonCNH trace shows sharper/more distinct peaks than CNH(1:1) and CNH(3:1) in rendered Fig. S1——Visual Estimate
Qualitative		SI p.2 · Supplementary figures · Fig. S1

Powder X-ray diffraction

X-ray diffraction and scattering

CNH (3:1) as-synthesised powder · Powder

Supplementary XRD pattern for CNH(3:1) in the Co/Ni-ratio comparison.

Context
ratio-variant pristine framework
Measurement source
SI p.2 · Supplementary figures · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Powder X-ray diffraction

X-ray diffraction and scattering

CH as-synthesised powder · Powder

Rigaku D/Max-3A, Cu Kalpha radiation, scan rate 8 min^-1; compared with simulated CH pattern.

Context
pristine framework control
Measurement source
p.3-p.4 · Physical characterization; Results · Fig. 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CH crystallization rate4.58%——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a

Powder X-ray diffraction

X-ray diffraction and scattering

CNH as-synthesised powder · Powder

Rigaku D/Max-3A, Cu Kalpha radiation, scan rate 8 min^-1; compared with CH and simulated pattern.

Context
target pristine framework
Measurement source
p.4 · Results and discussion · Fig. 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CNH crystallization rateMarked as a best value within this paper14.49%——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a
CNH XRD peak, (004)26.77 deg 2theta——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a
CNH XRD peak, (020)9.22 deg 2theta——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a
CNH XRD peak, (022)16.2 deg 2theta——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a
CNH XRD peak, (032)19.24 deg 2theta——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a
CNH XRD peak, (121)13.9 deg 2theta——Text
Exact Reported		p.4 · Results and discussion · Fig. 2a